Method for preparing antibacterial high-temperature-resistant plastic granules
A technology of plastic particles and high temperature resistance, which is used in the preparation of high temperature plastic particles and antibacterial fields.
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Embodiment 1
[0032] A preparation method of antibacterial and high temperature resistant plastic particles includes the following steps:
[0033] (1) Raw material pretreatment:
[0034] Put the general-purpose plastic resin in a vacuum drying box for drying treatment, after drying to a moisture content of 0.3%, take out the general-purpose plastic resin for use;
[0035] (2) Ion implantation treatment:
[0036] Place the general plastic resin obtained in step (1) in a MEVVA source high-current ion implanter, use copper ions as the implanted element for ion implantation, and perform copper ion implantation for later use;
[0037] (3) Preparation of modified filler:
[0038] a. Put the hollow microspheres and dysprosium sulfate into a bead mill at a weight ratio of 5:0.4 for grinding, and after grinding at 2000 rpm for 10 minutes, mixed powder A is obtained for use;
[0039] b. Immerse the mixed powder A obtained in operation a in a 0.4% hydrochloric acid solution, and after stirring for 23 minutes at a...
Embodiment 2
[0055] A preparation method of antibacterial and high temperature resistant plastic particles includes the following steps:
[0056] (1) Raw material pretreatment:
[0057] Put the general-purpose plastic resin in a vacuum drying box for drying treatment, after drying to a moisture content of 0.4%, take out the general-purpose plastic resin for use;
[0058] (2) Ion implantation treatment:
[0059] Place the general plastic resin obtained in step (1) in a MEVVA source high-current ion implanter, use copper ions as the implanted element for ion implantation, and perform copper ion implantation for later use;
[0060] (3) Preparation of modified filler:
[0061] a. Put hollow microspheres and dysprosium sulfate into a bead mill at a weight ratio of 5.5:0.5 for grinding, and after grinding at 2500rpm for 13 minutes, mixed powder A is obtained for use;
[0062] b. Immerse the mixed powder A obtained in operation a in a 0.45% hydrochloric acid solution, stir at 245rpm for 25min under the condi...
Embodiment 3
[0078] A preparation method of antibacterial and high temperature resistant plastic particles includes the following steps:
[0079] (1) Raw material pretreatment:
[0080] Put the general-purpose plastic resin in a vacuum drying box for drying treatment, after drying to a moisture content of 0.5%, take out the general-purpose plastic resin for use;
[0081] (2) Ion implantation treatment:
[0082] Place the general plastic resin obtained in step (1) in a MEVVA source high-current ion implanter, use copper ions as the implanted element for ion implantation, and perform copper ion implantation for later use;
[0083] (3) Preparation of modified filler:
[0084] a. Put the hollow microspheres and dysprosium sulfate into a bead mill at a weight ratio of 6:0.6 for grinding, and after grinding at 3000 rpm for 16 minutes, mixed powder A is obtained for use;
[0085] b. Dip the mixed powder A obtained in operation a into a 0.5% hydrochloric acid solution, and after stirring for 27 minutes at 260...
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