High-temperature-resistant insulation coating and preparation method thereof
A technology of insulating coatings and high temperature resistance, applied in the direction of anti-corrosion coatings, coatings, etc., to achieve the effect of good surface smoothness, not easy to precipitate, and strong adhesion
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[0031] (1) Preparation of phosphate solution: phosphoric acid solution and metal hydroxide are placed in a reaction vessel and mixed and heated to a boiling state for reaction until the reaction system becomes transparent and the transparency no longer increases; then, the reaction system is cooled to room temperature, and aging at room temperature for more than 12 hours, preferably aging for 12 hours to 36 hours, to obtain a phosphate solution;
[0032] (2) Preparation of high temperature resistant insulating coating: add spherical powder, diluent and optional boric acid into the phosphate solution, mix the materials by ball milling for more than 2 hours after stirring evenly, preferably ball milling for 2 hours to 8 hours, Thus the high temperature resistant insulating coating is obtained.
Embodiment 1
[0035] Embodiment 1: Preparation of aluminum phosphate salt solution
[0036] Weigh 230g of 85% concentration phosphoric acid, Al(OH) 3 50g of the powder was placed in a reaction vessel and stirred evenly. Stir the reaction and heat up to boiling state, stop heating after the reaction system is transparent. The reaction system was cooled to room temperature and aged for 12 hours.
Embodiment 2
[0037] Embodiment 2: preparation magnesium phosphate salt and aluminum phosphate salt solution
[0038] Weigh 290g of 85% concentrated phosphoric acid, Al(OH) 3 Powder 50g, Mg(OH) 2 15g of powder, placed in a reaction vessel and stirred evenly. Stir the reaction and heat up to boiling state, stop heating after the reaction system is transparent. The reaction system was cooled to room temperature and aged for 16 hours.
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