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Process for preparing rapeseed oil by microwave method

A technology of rapeseed oil and microwave method, which is applied in the directions of fat oil/fat production, fat oil/fat refining, fat production, etc., can solve the problems of low yield of clear oil and difficulty in extraction, etc. The effect of demulsification rate

Inactive Publication Date: 2018-10-23
镇江虎瑞生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, the important problem faced in the process of preparing rapeseed oil by aqueous enzyme method is that most of the oil is tightly combined with protein in the form of emulsion, so it is difficult to extract, and the yield of clear oil is low.

Method used

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  • Process for preparing rapeseed oil by microwave method
  • Process for preparing rapeseed oil by microwave method
  • Process for preparing rapeseed oil by microwave method

Examples

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Effect test

Embodiment 1

[0024] A process for preparing rapeseed oil by a microwave method, comprising the following steps: (1) seed selection: select plump rapeseeds without mildew, and use coarse and fine sieves to remove silt, dust and other sundries on the rapeseeds; (2) Crush: Dry grind the rapeseeds to 15 meshes and set aside; (3) Soak: Mix the crushed rapeseeds with water and cook them; (4) Ultrasonic: After drying the water at room temperature, mix them with water and carry out Ultrasonic treatment; (5) Enzyme addition: Add enzyme solution to the rapeseed mixture, mix well; (6) Alkaline extraction: adjust the mixture to alkaline, heat up for alkaline extraction; (7) Hydrolysis: add protease for hydrolysis ; (8) high temperature enzyme; (9) centrifugal separation, suck out the upper layer of grease; (10) add water to the lower layer of the emulsion and mix it, and then perform ultrasonic treatment again; (11) adjust the mixed solution to acidity; (12) segmental vacuum Microwave treatment: trans...

Embodiment 2

[0042] A process for preparing rapeseed oil by a microwave method, comprising the following steps: (1) seed selection: select plump rapeseeds without mildew, and use coarse and fine sieves to remove silt, dust and other sundries on the rapeseeds; (2) Crush: Dry grind the rapeseeds to 10 meshes and set aside; (3) Soak: Mix the crushed rapeseeds with water and cook them; (4) Ultrasonic: After drying the water at room temperature, mix them with water and carry out Ultrasonic treatment; (5) Enzyme addition: Add enzyme solution to the rapeseed mixture, mix well; (6) Alkaline extraction: adjust the mixture to alkaline, heat up for alkaline extraction; (7) Hydrolysis: add protease for hydrolysis ; (8) high temperature enzyme; (9) centrifugal separation, suck out the upper layer of grease; (10) add water to the lower layer of the emulsion and mix it, and then perform ultrasonic treatment again; (11) adjust the mixed solution to acidity; (12) segmental vacuum Microwave treatment: trans...

Embodiment 3

[0059] A process for preparing rapeseed oil by a microwave method, comprising the following steps: (1) seed selection: select plump rapeseeds without mildew, and use coarse and fine sieves to remove silt, dust and other sundries on the rapeseeds; (2) Crush: Dry grind the rapeseed to 20 meshes, and set aside; (3) Soak: Mix the crushed rapeseed with water, and cook; (4) Ultrasonic: After drying the water at room temperature, mix it with water, and carry out Ultrasonic treatment; (5) Enzyme addition: Add enzyme solution to the rapeseed mixture, mix well; (6) Alkaline extraction: adjust the mixture to alkaline, heat up for alkaline extraction; (7) Hydrolysis: add protease for hydrolysis ; (8) high temperature enzyme; (9) centrifugal separation, suck out the upper layer of grease; (10) add water to the lower layer of the emulsion and mix it, and then perform ultrasonic treatment again; (11) adjust the mixed solution to acidity; (12) segmental vacuum Microwave treatment: transfer th...

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Abstract

The invention discloses a process for preparing rapeseed oil by a microwave method. The process comprises the following steps of (1) seed selection; (2) crushing; (3) soaking; (4) ultrasound treatment; (5) enzyme addition; (6) alkaline extraction; (7) hydrolysis; (8) high-temperature enzyme deactivation; (9) centrifugal separation, and upper layer grease suction; (10) water adding uniform mixing on lower layer emulsion, and secondary ultrasound treatment; (11) mixed liquid regulation to the acid state; (12) segmented vacuum microwave treatment; (13) centrifugation and rapeseed clear oil obtaining. In the process of preparing the rapeseed oil, the twice grease extraction is performed; the clear oil yield is effectively improved; the ultrasound is used for assisting the water enzyme method to process the rapeseeds; the duplex effects of the ultrasound and the enzyme are utilized; the plant cell structure is damaged; the moisture in the rapeseeds is fast vaporized; the dissolute-out of the grease micro particles in the rapeseeds and the formation of porous structures inside plant tissues can be promoted; the oil yield is improved; the ultrasound assisted segmented microwave method isused for performing demulsification process on emulsion generated in the rapeseed oil process by the ultrasound assisted segmented microwave method; the demulsification rate is improved; the high clear oil yield is further improved.

Description

technical field [0001] The invention belongs to the field of vegetable oil processing, in particular to a process for preparing rapeseed oil by a microwave method. Background technique [0002] Rapeseed is an important oil crop in the world, and its output ranks fourth in the world, after soybean, cottonseed and palm. In my country, the planting area and output of rapeseed rank first in the world. As an important oil crop, it is also a crop high in high-quality vegetable protein. The traditional extraction methods of rapeseed oil are pressing and extraction. Among them, the extraction method has been controversial all over the world due to the use of organic solvents such as n-hexane. The organic solvent used in the solvent extraction method not only has a destructive effect on the atmospheric environment, but is also flammable, explosive and extremely unsafe, which endangers the production safety of oil production enterprises. The pressing method not only has a lower oil...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B1/02C11B1/04C11B1/10C11B3/00C11B3/06C11B3/16
CPCC11B1/025C11B1/04C11B1/106C11B1/108C11B3/001C11B3/003C11B3/005C11B3/06C11B3/16
Inventor 王俗新王月阳
Owner 镇江虎瑞生物科技有限公司
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