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Method for preparing Cu-doped indium-oxide nanowire based on regulable porous silicon substrate

A technology of porous silicon and indium oxide, applied in chemical instruments and methods, nanotechnology for materials and surface science, nanotechnology, etc., can solve the problems of uneven catalyst, high temperature, uncontrollable distribution and size, etc. Combines a strong effect

Inactive Publication Date: 2018-08-07
TIANJIN UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

1. The reaction temperature is high, and the deposition rate is very low, about a few microns or hundreds of microns per hour
2. The gas flow rate of the carrier gas is difficult to control, and the reactants cannot be accurately deposited on the required position on the substrate, and the diameter of the nanowire has too many controllable variables to determine the accurate process parameters
3. The samples of nanowires grown on silicon substrates are not uniform due to the use of catalysts, and the distribution and size of the reaction process cannot be controlled, so the shape of the grown nanowires is irregular, uneven and easy to form clusters

Method used

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  • Method for preparing Cu-doped indium-oxide nanowire based on regulable porous silicon substrate
  • Method for preparing Cu-doped indium-oxide nanowire based on regulable porous silicon substrate

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Embodiment 1

[0018] The present invention will be further described below in conjunction with the accompanying drawings.

[0019] A method for preparing Cu-doped indium oxide nanowires based on an adjustable porous silicon substrate, the main steps of which are as follows;

[0020] 1) Choose a (100) pure silicon wafer polished on one side as the substrate, pre-design the hole distribution, hole diameter and depth of the silicon substrate, choose diamond sandpaper that is similar to or slightly smaller than the hole size required, and use The method of mechanical grinding prefabricates several grooves matching the hole width of the porous silicon on the surface of the silicon substrate, and the arrangement of the grooves is consistent with the hole distribution of the porous silicon;

[0021] 2) Configure the mixed solution of dimethylformamide and hydrofluoric acid as the electrochemical reaction solution according to the volume ratio of 1:3.5, put the silicon substrate with grooves on the...

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Abstract

The invention discloses a method for preparing a Cu-doped indium-oxide nanowire based on a regulable porous silicon substrate. With a CVD method, an indium-oxide nanowire is prepared; and a substratematerial is processed to prepare a porous substrate with the uniform surface, so that a nanowire structure with a regular array is made. With the method disclosed by the invention, the holes in the substrate surface can be adjusted based on the needed condition; and the hole distribution and hole dimensions are changed and catalyst gold is injected into the holes, so that the nanowire growth / distribution / dimension is regulated. Therefore, nano-particle and block generation during the preparation process is reduced effectively; the prepared nanowire can be bonded to the substrate firmly; and thus the prepared Cu-doped indium-oxide nanowire has the great actual application value.

Description

technical field [0001] The invention relates to a method for preparing a Cu-doped indium oxide nanometer material, belonging to the field of nanometer material preparation. Background technique [0002] Indium oxide nanomaterials have gradually become a research hotspot in wide bandgap semiconductor nanomaterials due to their wide bandgap, good conductivity, low electron affinity, high breakdown electric field and better chemical stability. Devices, gas sensors, solar panels and displays have good application prospects. In recent years, people have made some progress in the preparation and performance research of indium oxide nanomaterials. Researchers have prepared various nanostructures of indium oxide materials through a variety of physical and chemical methods, and corresponding progress has been made in the field of research on the luminescence properties of indium oxide nanostructures, but there are still many issues that need to be further studied. At the same time,...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01L21/02C01G15/00B82Y30/00B82Y40/00
CPCB82Y30/00B82Y40/00C01G15/00C01P2002/54C01P2004/03C01P2004/16H01L21/02381H01L21/0243H01L21/02565H01L21/0257H01L21/02603H01L21/0262
Inventor 刘技文温帅
Owner TIANJIN UNIVERSITY OF TECHNOLOGY
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