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Leveling agent and preparation method thereof

A technology of leveling agent and hydromica, which is applied in the field of textile materials, can solve the problems of poor dye applicability, high price, and adverse effects of dyeing light fastness, and achieve uniform dyeing and good level dyeing effect

Inactive Publication Date: 2018-04-13
SUZHOU INST OF TRADE & COMMERCE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the disadvantages of these two types of leveling agents are poor applicability to different types of dyes, adverse effects on light fastness of dyeing, and higher prices

Method used

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  • Leveling agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A leveling agent prepared from the following ingredients in parts by weight: 2 parts of hydromica, 1 part of spherical nano-titanium dioxide, 2 parts of halloysite, 2 parts of sodium bentonite, 2 parts of sodium fluorosilicate, and sodium caseinate 2 parts, sodium selenate 2 parts, sodium ferulate 1 part, sodium lauryl sulfate 2 parts, talc powder 1 part, polyvinyl alcohol 3 parts, xylitol 2 parts, N-methylpyrrolidone 1 part, diacetyl 3 parts of monoglyceride tartrate, 2 parts of sodium stearoyl lactylate, 3 parts of ylang-ylang oil, 4 parts of isopropanol, 150 parts of deionized water.

[0019] The preparation method of above-mentioned leveling agent is:

[0020] (1) Mix hydromica, halloysite, talcum powder, sodium bentonite and isopropanol, and grind for 10 hours with a grinder;

[0021] (2) Wash with water, filter and dry in an oven at a temperature of 90°C;

[0022] (3) Pass through a 200-mesh sieve to remove large particles;

[0023] (4) Mix with sodium fluorosi...

Embodiment 2

[0027] A leveling agent prepared from the following components in parts by weight: 3 parts of hydromica, 1.2 parts of spherical nano-titanium dioxide, 3 parts of halloysite, 3 parts of sodium bentonite, 3 parts of sodium fluorosilicate, and sodium caseinate 3 parts, 2.5 parts of sodium selenate, 1.5 parts of sodium ferulate, 3 parts of sodium lauryl sulfate, 1.5 parts of talcum powder, 4 parts of polyvinyl alcohol, 2.5 parts of xylitol, 1.5 parts of N-methylpyrrolidone, diacetyl 4 parts of monoglyceride tartrate, 3 parts of sodium stearoyl lactylate, 4 parts of ylang-ylang oil, 5 parts of isopropanol, 200 parts of deionized water.

[0028] The preparation method of above-mentioned leveling agent is:

[0029] (1) Mix hydromica, halloysite, talcum powder, sodium bentonite and isopropanol, and grind for 11 hours with a grinder;

[0030] (2) Wash with water, filter and dry in an oven at a temperature of 95°C;

[0031] (3) Pass through a 200-mesh sieve to remove large particles; ...

Embodiment 3

[0036] A leveling agent, which is prepared from the following components in parts by weight: 3.5 parts of hydromica, 1.5 parts of spherical nano-titanium dioxide, 3.5 parts of halloysite, 3.5 parts of sodium bentonite, 3.5 parts of sodium fluorosilicate, and sodium caseinate 3.5 parts, 3 parts of sodium selenate, 1.5 parts of sodium ferulate, 3 parts of sodium lauryl sulfate, 1.5 parts of talcum powder, 4.5 parts of polyvinyl alcohol, 3 parts of xylitol, 1.5 parts of N-methylpyrrolidone, diacetyl 5 parts of monoglyceride tartrate, 3.5 parts of sodium stearoyl lactylate, 4.5 parts of ylang-ylang oil, 6 parts of isopropanol, and 200 parts of deionized water.

[0037] The preparation method of above-mentioned leveling agent is:

[0038] (1) Mix hydromica, halloysite, talcum powder, sodium bentonite and isopropanol, and grind for 11 hours with a grinder;

[0039] (2) Wash with water, filter and dry in an oven at a temperature of 95°C;

[0040] (3) Pass through a 200-mesh sieve t...

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Abstract

The invention provides a leveling agent and a preparation method thereof. The preparation method comprises the following steps: (1) mixing hydromica, halloysite, talcum powder, sodium bentonite and isopropanol, and grinding the mixture; (2) washing the ground mixture with water, filtering and then drying; (3) screening the product with a 200-mesh sieve for removing large particles; (4) mixing thescreened product with sodium fluosilicate, sodium caseinate, sodium selenate, sodium ferulate, xylitol and deionized water, heating and stirring for carrying out a reaction; (5) putting the reaction products into a centrifugal machine for carrying out centrifugal separation, and removing supernatant; (6) adding spherical nano titanium dioxide, sodium lauryl sulfate, polyvinyl alcohol, N-methyl pyrrolidone, sodium stearoyl lactylate, diacetyl tartaric acid monoglyceride, fatty alcohol polyoxyethylene ether, ylang ylang oil and the remaining deionized water, and stirring at the high speed to obtain the leveling agent. The leveling agent provided by the invention is uniform in dyeing to fabric, good in level dyeing effect, and high in level of dry and wet rubbing fastness; furthermore, afterbeing washed with water, the leveling agent enables the color not to be changed basically, does not stain, and has very high fastness to washing.

Description

technical field [0001] The invention relates to the field of textile materials, in particular to a leveling agent and a preparation method thereof. Background technique [0002] Textile auxiliaries are very important to increase the added value of textiles. They can not only make textiles functional, but also make them upscale and more contemporary. However, the prerequisite for these advantages is that the dyeing of the fabric must be even and transparent. Leveling agent to achieve. Most leveling agents are water-soluble surfactants. According to the influence of leveling agents on dye diffusion and aggregation, they are mainly divided into two types: one is fibrophilic leveling agent, which has almost no effect on the aggregation of dyes. No effect, but the affinity for fibers is greater than that of dyes for fibers. Therefore, during the dyeing process, this type of leveling agent will first combine with fibers to reduce the dyeing rate of dyes. This type of leveling age...

Claims

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Application Information

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IPC IPC(8): D06P1/52D06P1/62D06P1/647D06P1/651D06P1/653D06P1/673
Inventor 张小英
Owner SUZHOU INST OF TRADE & COMMERCE
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