Preparation method of flame-retardant material for wires and cables
A flame-retardant material, wire and cable technology, applied in the field of flame-retardant materials, can solve the problem that flame-retardant materials cannot take into account flame-retardant performance, mechanical performance and environmental protection, etc., to ensure mechanical performance, improve flame retardancy, and good environmental protection Effect
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[0029] Embodiments of the present invention provide a method for preparing a wire and cable flame retardant material, comprising:
[0030] 1) Preparation of modified dopa polymer solution:
[0031] Using levodopa modified by benzyl chloroformate as a monomer, the modified dopa polymer is prepared through polymerization;
[0032] Dissolving the modified dopa polymer in acetone to prepare a modified dopa polymer solution;
[0033] 2) Preparation of sodium-based montmorillonite dispersion:
[0034] placing the sodium-based montmorillonite in an ethanol solution to prepare a sodium-based montmorillonite dispersion, and using an alkaline solution to adjust the pH value of the sodium-based montmorillonite dispersion to 9.5-10;
[0035] Using an ultrasonic cell pulverizer to treat the sodium-based montmorillonite dispersion for 7 to 9 minutes to obtain a uniformly dispersed sodium-based montmorillonite dispersion;
[0036] 3) Preparation of polyimide fiber substrate:
[0037] Soa...
Embodiment 1
[0043] A method for preparing a wire and cable flame retardant material, comprising:
[0044] 1) Preparation of modified dopa polymer solution:
[0045] With levodopa modified by benzyl chloroformate as a monomer, a modified dopa polymer is obtained through a polymerization reaction, and the molecular weight of the modified dopa polymer obtained is at least 6000 g / mol;
[0046] Dissolving the modified dopa polymer in acetone to prepare a modified dopa polymer solution, the concentration of the prepared modified dopa polymer solution is respectively 0.02wt%;
[0047] 2) Preparation of sodium-based montmorillonite dispersion:
[0048] The sodium-based montmorillonite is placed in an ethanol solution with a concentration of 50% V / V to make a sodium-based montmorillonite dispersion, and the concentration of the prepared sodium-based montmorillonite dispersion is 0.22wt%. The NaOH solution of 1 adjusts the pH value of the sodium-based montmorillonite dispersion to 9.5;
[0049] ...
Embodiment 2
[0057] A method for preparing a wire and cable flame retardant material, comprising:
[0058] 1) Preparation of modified dopa polymer solution:
[0059] With levodopa modified by benzyl chloroformate as a monomer, a modified dopa polymer is obtained through polymerization, and the molecular weight of the modified dopa polymer obtained is as large as 6300g / mol;
[0060] Dissolving the modified dopa polymer in acetone to prepare a modified dopa polymer solution, the concentration of the prepared modified dopa polymer solution is respectively 0.06wt%;
[0061] 2) Preparation of sodium-based montmorillonite dispersion:
[0062] The sodium-based montmorillonite is placed in an ethanol solution with a concentration of 53% V / V to make a sodium-based montmorillonite dispersion, and the concentration of the prepared sodium-based montmorillonite dispersion is 0.24wt%. adjusting the pH value of the sodium-based montmorillonite dispersion to 9.7 with a 1.2M NaOH solution;
[0063] Using ...
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