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Camellia oleifera fruit phase separation process

A process method, the technology of camellia oleifera fruit, which is applied in the fields of petroleum industry, fat oil/fat production, fat oil/fat refining, etc., can solve the problems of high moisture requirement of oil raw materials, decreased nutritional value, hidden safety hazards, etc., and achieves the improvement of edible palatability and Eating safety, high oil quality, and the effect of saving production man-hours

Pending Publication Date: 2017-12-22
湖南大三湘油茶生态产业有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, the pressing method, solvent leaching method and supercritical fluid extraction method have high requirements on the moisture of the oil raw material. When the moisture is low to a certain range, the oil yield of the oil can reach a high level; the aqueous enzymatic method is to fine the oil raw material and add water to adjust the pH Then add biological enzymes to extract the oil under certain conditions. The oil raw materials are crushed as finely as possible, and the moisture requirements of the oil raw materials are also high; and people control the moisture of the oil raw materials through natural drying and then mechanical drying. The moisture control process requires a long period; fresh tea fruit leaves the parent body after picking, and internal consumption of nutrients occurs, and the oil quality decreases during the moisture control process, and subsequent degumming, deacidification, decolorization, deodorization and winterization of oil may be required Refining, which not only causes a decrease in nutritional value, but also creates more or less potential safety hazards

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] Take 1,000 kg of selected fresh tea fruits, and remove the husks through a sheller (the proportion of husks in fresh tea seeds is less than 1%) to obtain fresh tea seeds, which are then washed and crushed (the sieve diameter of the grinder is 3mm) ), crushed fresh camellia seed granules were squeezed (0.1 mm gap between the squeezing slots) to obtain solid fiber powder and whey, the whey moisture content was 40%, after heating to 65°C, add 9 mL of anhydrous per 40 g of whey The ratio of ethanol is to add absolute ethanol to the system, release the pressure after melting for 30 minutes at a pressure of 0.1 MPa, continue stirring and heating for 1 hour, and centrifuge for 5 minutes at a centrifuge speed of 1000 rpm to collect the light phase camellia oil. Put it at a temperature of 80°C and a vacuum of -0.09MPa for solvent recovery for 1.5 hours to obtain ethanol-free camellia oil, add activated carbon with 0.5% of the mass of the ethanol-free camellia oil, adsorb at a tem...

Embodiment 2

[0039] Take 1,000 kg of selected fresh tea fruits, remove the husks through a sheller (the proportion of husks in fresh tea seeds is less than 1%), and obtain fresh tea seeds, which are then washed and crushed (the sieve diameter of the grinder is 5mm) ), crushed fresh Camellia oleifera granules were squeezed (gap 0.3mm) to obtain whey, whey moisture content 60%, after heating to 70°C, add 15mL80% ethanol aqueous solution for every 40g whey Add 80% ethanol aqueous solution to the system, let it melt for 40 minutes at a pressure of 0.1 MPa, then release the pressure, continue stirring and heating for 50 minutes, centrifuge for 4 minutes at a centrifuge speed of 3000 rpm, collect the light phase camellia oil, and place the light phase camellia oil at a temperature of 80 ℃, vacuum degree -0.09MPa, carry out solvent recovery for 1.5 hours to obtain camellia oil without ethanol, add activated carbon with 1.0% of the mass of camellia oil without ethanol, adsorb at a temperature of 0°...

Embodiment 3

[0041] Take 1,000 kg of selected fresh tea fruit, remove the husk through a sheller (the proportion of husk in fresh tea seeds is less than 1%), and obtain fresh tea seeds, which are then washed and crushed (the sieve diameter of the grinder is 6mm) ), crushed fresh camellia oleifera granules were squeezed (the gap between the squeeze gaps was 1mm) to obtain whey, the whey content of whey was 45%, after heating to 60°C, add 12mL of 90% ethanol aqueous solution to the system according to the ratio of every 40g of whey Add 90% ethanol aqueous solution, melt at a pressure of 0.2 MPa for 50 minutes, release the pressure, continue stirring and heating for 50 minutes, centrifuge at a centrifuge speed of 5000 rpm for 3 minutes, collect the light phase camellia oil, and place the light phase camellia oil at a temperature of 80 ° C. The solvent was recovered for 75 minutes at a vacuum degree of -0.09MPa to obtain ethanol-free camellia oil, which was added with activated carbon of 1.5% o...

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PUM

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Abstract

A camellia oleifera fruit phase separation process comprises: (1) selection, which includes selecting newly-picked fresh plump camellia oleifera fruits; (2) hulling, which includes hulling the camellia oleifera fruits to obtain fresh plump camellia oleifera seeds; (3) washing, which includes washing the camellia oleifera seeds obtained from the step (2) with water; (4) pulverization, which includes putting the camellia oleifera seeds obtained from the step (3) to a pulverizer to obtain camellia oleifera seed granules; (5) phase separation 1, which includes putting the camellia oleifera seed granules obtained from the step (4) to a juice extractor, and performing extruding to obtain solid fiber powder and liquid whey; (6) medium separation, which includes sending the whey obtained from the step (5) to a reaction pot, performing heating, adding a medium, and performing continuous stirring and heating for layering; (7) phase separation 2, which includes centrifuging the emulsion obtained from step (6) to obtain light-phase camellia oil, a heavy-phase tea saponin solution, solid-phase protein, and a starch mixture; and (8) cold extraction. The process is simple in steps and high in oil yield, allows a lot of nutrients to be kept, and fully utilizes the camellia oleifera fruits.

Description

technical field [0001] The invention relates to the processing of oilseed fruit, in particular to a process method of phase separation of camellia oleifera fruit. Background technique [0002] Camellia oleifera is a plant of the genus Camellia in the family Theaceae. Camellia oleifera seed is the seed of the camellia oleifera tree. Camellia oil (also known as camellia seed oil, camellia oil, camellia oleifera oil) can be obtained by leaching or pressing. Camellia oil is a healthy and delicious edible oil. It is not only good in color, fragrance and taste, but also has the effect of preventing cardiovascular diseases such as hypertension, coronary heart disease and atherosclerosis, and has important development and utilization value. [0003] At present, the production methods of camellia oil mainly include pressing method, solvent leaching method, aqueous enzymatic method, supercritical fluid extraction method and so on. Among them, the pressing method, solvent leaching met...

Claims

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Application Information

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IPC IPC(8): C11B1/06C11B1/04C11B3/10C10L5/44
CPCC10L5/445C11B1/04C11B1/06C11B3/10Y02E50/10Y02E50/30
Inventor 谭传波杨耀学赖琼玮邓一军刘芳凌小辉罗秋兰黄闺李元军李志成肖春生
Owner 湖南大三湘油茶生态产业有限公司
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