A kind of preparation method of granite polishing powder
A technology for polishing powder and granite, applied in chemical instruments and methods, polishing compositions containing abrasives, and other chemical processes, etc., can solve the problems of polishing powder concentration changes, affecting polishing efficiency, changes, etc., and achieving a small number of scratches , The effect of less dosage and easy control of conditions
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Embodiment 1
[0020] (1) ZrN-CeO 2 -SiO 2 Preparation of the complex: Add water: 40 mL, cerium chloride: 28 g, zirconium nitride: 18 g, silicon dioxide: 10 g to the reactor, stir and dissolve, add ammonia water: 4 mL, stir at room temperature for 40 min, Solid-liquid separation, dried at 100±2°C, then roasted at 850±10°C for 2 hours, cooled, and crushed by airflow to obtain light yellow ZrN-CeO 2 -SiO 2 Complex;
[0021] (2) Preparation of granite polishing powder: In the grinder, add ZrN-CeO 2 -SiO 2 Compound: 25g, oxalic acid dihydrate: 12g, sodium oxalate: 18g, grind, mix well, add ammonium fluorozirconate: 22g, palmitic acid: 21g, grind, mix well, paraffin powder: 2g, grind, mix well, that is Get light yellow granite polishing powder.
Embodiment 2
[0023] (1) ZrN-CeO 2 -SiO 2 Preparation of the compound: Add water: 400 mL, cerium chloride: 280 g, zirconium nitride: 180 g, silicon dioxide: 100 g to the reactor, stir and dissolve, add ammonia water: 40 mL, stir at room temperature for 40 min, Solid-liquid separation, dried at 100±2°C, then roasted at 850±10°C for 2 hours, cooled, and crushed by airflow to obtain light yellow ZrN-CeO 2 -SiO 2 Complex;
[0024] (2) Preparation of granite polishing powder: In the grinder, add ZrN-CeO 2 -SiO 2 Compound: 250g, oxalic acid dihydrate: 120g, sodium oxalate: 180g, grind, mix well, add ammonium fluozirconate: 220g, palmitic acid: 210g, grind, mix well, paraffin powder: 20g, grind, mix well, that is Get light yellow granite polishing powder.
Embodiment 3
[0026] (1) ZrN-CeO 2 -SiO 2 Preparation of the complex: Add water: 220 mL, cerium chloride: 125 g, zirconium nitride: 100 g, silicon dioxide: 40 g to the reactor, stir and dissolve, add ammonia water: 15 mL, and stir at room temperature for 40 minutes. Solid-liquid separation, dried at 100±2°C, then roasted at 850±10°C for 2 hours, cooled, and crushed by airflow to obtain light yellow ZrN-CeO 2 -SiO 2 Complex;
[0027] (2) Preparation of granite polishing powder: In the grinder, add ZrN-CeO 2 -SiO 2 Compound: 108g, oxalic acid dihydrate: 75g, sodium oxalate: 75g, grind, mix well, add ammonium fluozirconate: 120g, palmitic acid: 100g, grind, mix well, paraffin powder: 20g, grind, mix well, that is Get light yellow granite polishing powder.
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