Low-remanence nanocrystalline magnetic core and preparation method thereof
A nanocrystalline, low remanence technology, which is applied in the manufacture of inductors/transformers/magnets, magnetic materials, magnetic objects, etc., can solve the problems of high remanence, limited application range, and high production cost of iron-based nanocrystalline cores, and achieve Improve the saturation magnetic induction intensity, increase the quality factor, and reduce the effect of loss value
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Embodiment 1
[0053] A preparation method of a nanocrystalline magnetic core with low remanence, comprising the steps of:
[0054] (1) Vacuum isothermal annealing of the iron-nickel-based nanocrystalline strips prepared by the single-roller melt rotary rapid quenching method at a temperature of 450°C and a vacuum degree of 0.0005Pa for 1h, then furnace cooling to 250°C, and holding for 0.5h. Then water cooled to room temperature;
[0055] (2) Crushing the iron-nickel-based nanocrystalline strip to obtain nanocrystalline metal powder, performing ball milling on the nanocrystalline metal powder, and sieving into 70% of the first powder passing through -200 mesh and 30% of the first powder passing through -150~+200 mesh second powder;
[0056] (3) Take the first powder and add an appropriate amount of water to prepare a suspension with a mass fraction of 30%, then add the first insulating coating agent, stir evenly, disperse ultrasonically for 15 minutes, filter, dry, crush and grind until th...
Embodiment 2
[0082] A preparation method of a nanocrystalline magnetic core with low remanence, comprising the steps of:
[0083] (1) Vacuum isothermal annealing of the iron-nickel-based nanocrystalline strips prepared by the single-roller melt rotary rapid quenching method at a temperature of 460°C and a vacuum degree of 0.0008Pa for 1.2h, cooled to 280°C in the furnace, and kept for 0.8h , and then water cooled to room temperature;
[0084] (2) Crushing the iron-nickel-based nanocrystalline strip to obtain nanocrystalline metal powder, performing ball milling on the nanocrystalline metal powder, and sieving into 75% of the first powder passing through -200 mesh and 25% of the first powder passing through -150~+200 mesh second powder;
[0085] (3) Take the first powder and add an appropriate amount of water to prepare a suspension with a mass fraction of 35%, then add the first insulating coating agent, stir evenly, disperse ultrasonically for 18 minutes, filter, dry, crush and grind to ...
Embodiment 3
[0111] A preparation method of a nanocrystalline magnetic core with low remanence, comprising the steps of:
[0112] (1) Vacuum isothermal annealing of the iron-nickel-based nanocrystalline strips prepared by the single-roller melt rotary rapid quenching method at a temperature of 475°C and a vacuum degree of 0.001Pa for 1.5h, then cooled to 300°C in the furnace, and kept for 1h. Then water cooled to room temperature;
[0113] (2) Crushing the iron-nickel-based nanocrystalline strip to obtain nanocrystalline metal powder, performing ball milling on the nanocrystalline metal powder, and sieving into 80% of the first powder passing through -200 mesh and 20% of the first powder passing through -150~+200 mesh second powder;
[0114] (3) Take the first powder and add an appropriate amount of water to prepare a suspension with a mass fraction of 40%, then add the first insulating coating agent, stir evenly, disperse ultrasonically for 20 minutes, filter, dry, crush and grind to a p...
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