Novel method for efficiently extractinganthocyanin from black rice
An anthocyanin and new method technology, applied in the field of food processing, can solve the problems of difficulty in popularization, low extraction efficiency, loss of anthocyanin, etc., and achieve the effects of protecting from damage, improving extraction yield, and promoting infiltration speed.
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Embodiment 1
[0025] A new method for efficiently extracting anthocyanins from black rice comprises steps of drying black rice raw material, ultrafine pulverization, solvent immersion, ultra-high pressure extraction, filtration and centrifugation, removal of ethanol, ion exchange resin purification, and freeze-drying steps.
Embodiment 2
[0027] A new method for efficiently extracting anthocyanins from black rice, comprising the steps of drying black rice raw materials, ultrafine pulverization, solvent immersion, ultra-high pressure extraction, filtration and centrifugation, removal of ethanol, ion exchange resin purification, and freeze-drying steps; Ultra-high pressure extraction adopts intermittent pressurized ultra-high pressure extraction. The specific steps are: transfer the solvent mixture of dispersed black rice powder into a high-pressure polyethylene bag, exhaust as much air as possible and seal it, and transfer it to the ultra-high pressure extraction equipment. Extract under the condition of 250-350MPa for 10-30min, then release the pressure, maintain the normal pressure state for 5-10min, then extract under the condition of 350-450MPa for 10-30min, after the extraction, collect the extract for later use.
Embodiment 3
[0029] 1) Drying of black rice raw material: drying the black rice raw material at 40-45°C until its moisture content is 13%-14%;
[0030] 2) Superfine pulverization: pulverize the original black rice material in a high-speed pulverizer to a particle size of 80-120 mesh to obtain black rice powder;
[0031] 3) Solvent immersion: take a certain amount of black rice powder, add ethanol solution with a mass concentration of 50% according to the mass ratio of material to liquid of 1:5-15kg / kg, use hydrochloric acid to adjust the pH of the solution to 2.5-3.5, and stir evenly;
[0032] 4) Ultra-high pressure extraction: transfer the solvent mixture of the dispersed black rice powder into a high-pressure polyethylene bag, exhaust as much air as possible and seal it, transfer it to the ultra-high pressure extraction equipment, and extract under the condition of 250-350MPa for 10-30 minutes, Then release the pressure and maintain the normal pressure state for 5-10 minutes, and then ex...
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