foundation waterproof structure
A technology for structures and foundations, which is applied to coagulating pavements, roads, bridges and other directions laid on site. It can solve the problems of slow drying, delayed construction period, poor adhesion between layers, etc., and achieve excellent adhesion and shorten construction. effect of time
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[0089] Hereinafter, the present invention will be described in more detail using examples.
Synthetic example 1
[0090] [Synthesis Example 1] Preparation of Moisture Curable Urethane Composition (ii-1) for Urethane Waterproofing Material
[0091] In a four-necked flask equipped with a thermometer, a stirrer, an inert gas inlet, and a reflux condenser, 1,000 parts by mass of polytetramethylene glycol (number average molecular weight: 1,000) and 297 parts by mass of dipropylene glycol were mixed, and 661 parts by mass of toluene diisocyanate was added thereto, and reacted at 90° C. for 8 hours under a nitrogen stream to obtain a urethane prepolymer having an NCO% of 2.5 mass % and a weight average molecular weight of 6,080.
[0092] Next, 100 parts by mass of polyoxyethylene polyoxypropylene diol (number average molecular weight: 1,000, content of oxyethylene structure: 20 mass %) and 80 parts by mass of toluene diisocyanate were reacted to obtain NCO% of 16.8 mass % Urethane prepolymer. Next, 40 parts by mass of xylene was added, and 114.5 parts by mass of N-2-isopropyl-3-(2-hydroxyethyl...
Synthetic example 2
[0095] [Synthesis Example 2] Preparation of Moisture Curing Type Urethane Primer (iii-1)
[0096] In a four-necked flask equipped with a thermometer, a stirrer, an inert gas inlet, and a reflux condenser, 300 parts by mass of crude MDI ("Millionate MR-200" manufactured by Nippon Polyurethane Industry Co., Ltd.), polypropylene glycol (number average molecular weight: 700) 210 parts by mass, 474 parts by mass of toluene, and 474 parts by mass of ethyl acetate were reacted at 80°C for 5 hours to obtain a moisture-curable urethane having a solid content of 35% by mass and an NCO% of 5.2% by mass Primer (iii-1).
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