Graphene-modified shell material and preparation method thereof
A technology of graphene modification and shell material, which is applied in the direction of additive processing, etc., and can solve the problem of poor heat dissipation of the laptop shell
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[0054] The preparation method of the shell material of described graphene modification, comprises the following steps:
[0055]S1: crush the PET resin and tris(2,4-di-tert-butylphenyl)phosphite and pass through a 200-300 mesh sieve to obtain mixed resin powder;
[0056] S2: adding a surfactant to the mixed resin powder prepared in step S1, and activating it for 1-1.3 hours at a temperature of 68-72° C. and a rotational speed of 150-180 r / min to prepare an activated mixed resin powder;
[0057] S3: Pulverize the graphene and pass it through a 200-300 mesh sieve to obtain a powder. The obtained powder is under a magnetic field strength of 7000-8200GS, an ultrasonic power of 520-650W, a temperature of 52-56°C, and a rotation speed of 200-300r / min. , stirring for 40-50min to obtain graphene energy powder;
[0058] S4: Under the protection of nitrogen, add the graphene energy powder prepared in step S3, polylactic acid, potassium tripolyphosphate, chloropropyl styrene, maleic anhy...
Embodiment 1
[0067] A graphene-modified shell material, in parts by weight, comprising the following raw materials: 3 parts of graphene, 106 parts of PBT resin, 30 parts of three (2,4-di-tert-butylphenyl) phosphite, poly 65 parts of lactic acid, 52 parts of potassium tripolyphosphate, 15 parts of chloropropyl styrene, 12 parts of maleic anhydride grafted polypropylene, 10 parts of sodium hydroxymethyl cellulose, 5 parts of Kevlar fiber, polyethylene terephthalic acid 4 parts of butylene glycol ester fiber, 1.3 parts of surfactant, 0.6 part of conditioner, 0.4 part of generating agent, 0.6 part of crosslinking agent, 1 part of compatibilizer, 0.7 part of bridging agent, 0.4 part of catalyst, 0.7 part of plasticizer 0.4 parts, 0.4 parts of dispersant, 0.6 parts of tackifier, 1.6 parts of curing agent, 0.4 parts of antioxidant, 0.3 parts of stabilizer, 1.5 parts of anti-aging agent, 2 parts of flame retardant;
[0068] The surfactant is polyoxyethylene-polyoxypropylene copolymer;
[0069] Th...
Embodiment 2
[0095] A graphene-modified shell material, in parts by weight, comprising the following raw materials: 1.6 parts of graphene, 80 parts of PBT resin, 21 parts of three (2,4-di-tert-butylphenyl) phosphite, poly 48 parts of lactic acid, 30 parts of potassium tripolyphosphate, 10 parts of chloropropyl styrene, 12 parts of maleic anhydride grafted polypropylene, 8 parts of sodium hydroxymethyl cellulose, 4 parts of Kevlar fiber, polyethylene terephthalic acid 3 parts of butanediol ester fiber, 1 part of surfactant, 0.4 part of regulator, 0.3 part of generating agent, 0.4 part of crosslinking agent, 0.7 part of compatibilizer, 0.5 part of bridging agent, 0.3 part of catalyst, 0.5 part of plasticizer 0.3 parts, 0.3 parts of dispersant, 0.4 parts of tackifier, 1 part of curing agent, 0.3 parts of antioxidant, 0.2 parts of stabilizer, 1.2 parts of anti-aging agent, 1.8 parts of flame retardant;
[0096] The surfactant is polyoxyethylene-polyoxypropylene copolymer;
[0097] The regulat...
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