Preparation method and application of efficient removing materials for interstitial water phosphate of sediments
A water phosphate and sediment technology, applied in chemical instruments and methods, water pollutants, water/sewage treatment, etc., can solve the problems of high phosphorus release risk and high ecological risk
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Embodiment 1
[0037] The sediment interstitial water phosphate efficient removal material described in this example is prepared by the following method:
[0038] (1) Collect lake sediments as raw materials, freeze-dry, grind and sieve to obtain sediment powders with a particle size of not less than 100 mesh, place the sediment powders in a muffle furnace at 450°C for 2 hours, and wait for After cooling to room temperature, use 0.2mol / L sodium hydroxide aqueous solution to wash with water, then place it in a blast drying oven and evaporate to dryness to obtain activated deposits, which are set aside;
[0039] (2) Take kaolin, dry, grind and sieve to obtain kaolin powder with a particle size of not less than 100 mesh, fully mix the activated sediment and kaolin powder in proportion to form a mixed powder, and the consumption of the kaolin accounted for 100% of the mixed powder. 75wt% of the total mass of the body, standby;
[0040] (3) Using 0.2mol / L FeSO 4 The aqueous solution is used to m...
Embodiment 2
[0043] The sediment interstitial water phosphate efficient removal material described in this example is prepared by the following method:
[0044] (1) Collect lake sediments as raw materials, freeze-dry, grind and sieve to obtain sediment powders with a particle size of not less than 100 mesh, place the sediment powders in a muffle furnace at 550°C for 1 hour, and wait for After cooling to room temperature, use 0.05mol / L sodium hydroxide aqueous solution to wash with water, then place it in a blast drying oven and evaporate to dryness to obtain activated deposits, which are set aside;
[0045] (2) Take kaolin, dry, grind and sieve to obtain kaolin powder with a particle size of not less than 100 mesh, fully mix the activated sediment and kaolin powder in proportion to form a mixed powder, and the consumption of the kaolin accounted for 100% of the mixed powder. 60wt% of the total mass of the body, spare;
[0046] (3) Using 0.2mol / L FeSO 4 The aqueous solution is used to mod...
Embodiment 3
[0049] The sediment interstitial water phosphate efficient removal material described in this example is prepared by the following method:
[0050] (1) Collect lake sediments as raw materials, freeze-dry, grind and sieve to obtain sediment powders with a particle size of not less than 100 mesh, place the sediment powders in a muffle furnace at 600°C for 2 hours, and wait for After cooling to room temperature, wash with 0.1 mol / L sodium hydroxide aqueous solution, then place in a blast drying oven and evaporate to dryness to obtain activated deposits, which are set aside;
[0051] (2) Take kaolin, dry, grind and sieve to obtain kaolin powder with a particle size of not less than 100 mesh, fully mix the activated sediment and kaolin powder in proportion to form a mixed powder, and the consumption of the kaolin accounted for 100% of the mixed powder. 50wt% of the total mass of the body, spare;
[0052] (3) Using 0.2mol / L FeSO 4 The aqueous solution is used to modify the mixed p...
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