Copper smelting converter tuyere brick and preparation method thereof
A copper-smelting converter and tuyere technology, which is applied in the field of refractory materials for copper-smelting converters, can solve problems such as reducing the volume stability of magnesia-alumina-titanium bricks, and achieve enhanced thermal shock resistance and volume stability, simple process, and slag corrosion resistance. strong effect
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Embodiment 1
[0033] A copper smelting converter tuyere brick and a preparation method thereof. Use 60~62wt% fused magnesia chrome sand particles as aggregate, 15~17wt% fused magnesia fine powder, 14~16wt% Cr 7 C 3 Fine powder, 5~7wt% zirconia micropowder and 1~2wt% yttrium oxide micropowder are base materials; The base material is added to the aggregate and mixed evenly. Then add zirconia sol accounting for 8~9wt% of the sum of the base material and the aggregate, mix evenly, press and form, cure at 25~30°C for 12~24h, and dry at 110~120°C 12~18h. Finally, place it in a muffle furnace, raise the temperature to 1550-1570°C at a heating rate of 4-5°C / min, keep it warm for 2-3 hours, and cool down with the furnace to make a copper smelting converter tuyere brick.
[0034] The copper smelting converter tuyere brick prepared in this example is measured: the cold compressive strength is 90~92MPa; the line change after burning is 0.10~0.12%; the 1450℃×3h static crucible method slag resistance...
Embodiment 2
[0036] A copper smelting converter tuyere brick and a preparation method thereof. Use 61~63wt% fused magnesia chrome sand particles as aggregate, 16~18wt% fused magnesia fine powder, 13~15wt% Cr 7 C 3Fine powder, 5~7wt% zirconia micropowder and 1~2wt% yttrium oxide micropowder are base materials; The base material is added to the aggregate and mixed evenly. Then add zirconia sol accounting for 8~9wt% of the sum of the base material and the aggregate, mix evenly, press and form, cure at 25~30°C for 12~24h, and dry at 110~120°C 12~18h. Finally, place it in a muffle furnace, raise the temperature to 1550-1570°C at a heating rate of 4-5°C / min, keep it warm for 2-3 hours, and cool down with the furnace to make a copper smelting converter tuyere brick.
[0037] The copper smelting converter tuyere brick prepared in this example is measured: the cold compressive strength is 91~93MPa; the line change after burning is 0.09~0.11%; the 1450℃×3h static crucible method slag resistance ...
Embodiment 3
[0039] A copper smelting converter tuyere brick and a preparation method thereof. With 62~64wt% fused magnesia chrome sand particles as aggregate, 17~19wt% fused magnesia fine powder, 12~14wt% Cr 7 C 3 Fine powder, 4~6wt% zirconia micropowder and 2~3wt% yttrium oxide micropowder are base materials; The base material is added to the aggregate and mixed evenly. Then add zirconia sol accounting for 9~10wt% of the sum of the base material and the aggregate, mix evenly, press and form, cure at 25~30°C for 12~24h, and dry at 110~120°C 12~18h. Finally, place it in a muffle furnace, raise the temperature to 1560-1580°C at a heating rate of 4-5°C / min, keep it warm for 2-3 hours, and cool down with the furnace to make a copper smelting converter tuyere brick.
[0040] The copper smelting converter tuyere brick prepared in this example is measured: the cold compressive strength is 92~94MPa; the line change after burning is 0.08~0.10%; the 1450℃×3h static crucible method slag resistan...
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