A kind of preparation method of bi‑2212 superconducting wire/tape
A bi-2212, superconducting wire technology, applied in the usage of superconducting elements, superconducting/high-conducting conductors, superconducting devices, etc., can solve the problems affecting the current-carrying performance of Bi-2212 wires/strips, ceramic powder in the center of wires Problems such as poor processing performance and broken core processing of multi-core wires can prevent poor processing uniformity, low manufacturing cost, and improve processing performance.
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Embodiment 1
[0022] The Bi-2212 superconducting wire / tape prepared in this embodiment is specifically a Bi-2212 superconducting wire, and the preparation method of the Bi-2212 superconducting wire includes the following steps:
[0023] Step 1. Place the Bi-2212 precursor powder in the heat treatment furnace, and then pass argon gas into the heat treatment furnace to remove the air in the furnace;
[0024] Step 2. Put the Bi-2212 precursor powder placed in the heat treatment furnace that has excluded the air in step 1. Under the protection of argon atmosphere, under the condition of oxygen partial pressure ≤ 50ppm, the temperature is raised to 400°C at a heating rate of 50°C / h and then kept. 3h, after cooling to room temperature of 25°C with the furnace, the pretreated Bi-2212 precursor powder is obtained; the superconducting transition temperature of the pretreated Bi-2212 precursor powder is not greater than 85K;
[0025] Step 3: Put the Bi-2212 precursor powder pretreated in step 2 into ...
Embodiment 2
[0031] The Bi-2212 superconducting wire / tape prepared in this embodiment is specifically a Bi-2212 superconducting wire, and the preparation method of the Bi-2212 superconducting wire includes the following steps:
[0032] Step 1. Place the Bi-2212 precursor powder in the heat treatment furnace, and then pass argon gas into the heat treatment furnace to remove the air in the furnace;
[0033] Step 2. Put the Bi-2212 precursor powder placed in the heat treatment furnace that has excluded the air in step 1. Under the protection of argon atmosphere, under the condition of oxygen partial pressure ≤ 50ppm, the temperature is raised to 500°C at a heating rate of 100°C / h and then kept. 2h, after cooling to room temperature of 25°C with the furnace, the pretreated Bi-2212 precursor powder is obtained; the superconducting transition temperature of the pretreated Bi-2212 precursor powder is not greater than 85K;
[0034]Step 3: Put the Bi-2212 precursor powder pretreated in step 2 into ...
Embodiment 3
[0040] The Bi-2212 superconducting wire / tape prepared in this embodiment is specifically a Bi-2212 superconducting wire, and the preparation method of the Bi-2212 superconducting wire includes the following steps:
[0041] Step 1. Place the Bi-2212 precursor powder in the heat treatment furnace, and then pass argon gas into the heat treatment furnace to remove the air in the furnace;
[0042] Step 2. Put the Bi-2212 precursor powder placed in the heat treatment furnace that has excluded the air in step 1. Under the protection of argon atmosphere, the oxygen partial pressure is ≤50ppm, and the temperature is raised to 450°C at a heating rate of 80°C / h and then kept. After 2.5 hours, the pretreated Bi-2212 precursor powder was obtained after cooling to room temperature of 25°C with the furnace; the superconducting transition temperature of the pretreated Bi-2212 precursor powder was not greater than 85K;
[0043] Step 3: Put the Bi-2212 precursor powder pretreated in step 2 into...
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