Preparation method and application of electrochemical chlordimeform sensor based on composite cerium-doped porous nanocomposite
A nano-composite material and insecticidal amidine technology, which is applied in the fields of material electrochemical variables, scientific instruments, analytical materials, etc., can solve the problems of low sensitivity, poor conductivity, and unfavorable practical application of electrochemical sensors, and improve the electron transfer ability. , the effect of improving strength and stability, and increasing the ability of electron transfer
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Embodiment 1
[0029] Example 1Ce-MoO 3 / TiO 2 g-C 3 N 4 preparation of
[0030] First, add 0.6mmol sodium molybdate and 0.8mmol cerium salt into 5mL tetrabutyl titanate, slowly add 0.5mL hydrofluoric acid during stirring, react in the reactor at 160°C for 24 hours, and cool to room temperature , after centrifuging and washing three times with ultrapure water and absolute ethanol, vacuum-dry at 50°C; secondly, take 150 mg of the dried solid and mix it with 400 mg of melamine, and grind it into powder; then, put the ground powder into a muffle furnace , the heating rate is 1°C / min, and it is calcined at 480°C for 5 hours; finally, the calcined powder is cooled to room temperature to obtain Ce-MoO 3 / TiO 2 g-C 3 N 4 ;
[0031] The cerium salt is cerium sulfate.
Embodiment 2
[0032] Example 2Ce-MoO 3 / TiO 2 g-C 3 N 4 preparation of
[0033] First, add 0.8mmol sodium molybdate and 1.0mmol cerium salt into 5mL tetrabutyl titanate, slowly add 0.65mL hydrofluoric acid during stirring, react in the reactor at 180°C for 21 hours, and cool to room temperature , washed with ultrapure water and absolute ethanol for three times, then vacuum-dried at 50°C; secondly, take 200mg of the dried solid and mix it with 400mg of melamine, and grind it into powder; then, put the ground powder into a muffle furnace , the heating rate is 2°C / min, and calcined at 520°C for 2 hours; finally, the calcined powder is cooled to room temperature to obtain Ce-MoO 3 / TiO 2 g-C 3 N 4 ;
[0034] The cerium salt is cerium chloride.
Embodiment 3
[0035] Example 3Ce-MoO 3 / TiO 2 g-C 3 N 4 preparation of
[0036] First, add 1.0mmol sodium molybdate and 1.2mmol cerium salt into 5mL tetrabutyl titanate, slowly add 0.8mL hydrofluoric acid during stirring, react in the reactor at 200°C for 18 hours, and cool to room temperature , after centrifuging and washing with ultrapure water and absolute ethanol three times, vacuum drying at 50°C; secondly, take 250 mg of the dried solid and mix it with 400 mg of melamine, and grind it into powder; then, put the ground powder into a muffle furnace , the heating rate was 3°C / min, and calcined at 560°C for 0.5 hours; finally, the calcined powder was cooled to room temperature to obtain Ce-MoO 3 / TiO 2 g-C 3 N 4 ;
[0037] The cerium salt is cerium nitrate.
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