Xuesaitong soft capsules and preparation and detecting methods thereof
A detection method and soft capsule technology, which is applied in capsule delivery, measuring devices, and pharmaceutical formulations, etc., can solve problems affecting the accuracy of the detection method, inaccurate dosage, large error range, etc., and achieve appropriate hardness and good quality stability , the effect of reducing the error
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Embodiment 1
[0025] Weigh 60kg of Panax notoginseng total saponins, 8kg of beeswax, 242kg of peanut oil and 20kg of palm oil, mix them evenly, and grind to obtain the contents; then weigh 220kg of medicinal gelatin, 99kg of glycerin, 1.76kg of white pigment, 0.308kg of ethylparaben, milk Mix 1.012kg of chocolate brown and 242kg of purified water, sol, filter, and stabilize the gel to obtain capsule skins; the contents and capsule skins are placed in a pilling device for pilling, drying, ball selection, polishing, and packaging. Specifications: 0.33g per capsule, each capsule contains 60mg of Panax notoginseng saponins.
Embodiment 2
[0027] Weigh 65kg of Panax notoginseng total saponins, 10kg of beeswax, 235kg of peanut oil, and 20kg of palm oil, mix them evenly, and grind to obtain the contents; then weigh 220kg of medicinal gelatin, 99kg of glycerin, 1.76kg of white pigment, 0.308kg of ethylparaben, milk Mix 1.012kg of chocolate brown and 242kg of purified water, sol, filter, and stabilize the gel to obtain capsule skins; the contents and capsule skins are placed in a pilling device for pilling, drying, ball selection, polishing, and packaging. Specifications: 0.33g per capsule, each capsule contains 60mg of Panax notoginseng saponins.
Embodiment 3
[0029] With the above-mentioned embodiment gained product waits for inspection as test sample.
[0030] [Content Determination] The total saponins of Panax notoginseng were determined by UV-Vis spectrophotometry (Appendix VA of Chinese Pharmacopoeia 2010 Edition).
[0031] Preparation of reference substance solution: Accurately weigh an appropriate amount of ginsenoside Re reference substance, add methanol to make a solution containing 1mg per 1ml.
[0032] Drawing of the standard curve: Precisely draw 0.3ml, 0.4ml, 0.5ml, 0.6ml, 0.7ml of the above solutions into 10ml volumetric flasks respectively, add methanol to dilute to the mark, shake well, precisely draw 2ml of the above-mentioned series of reference substance solutions, and place them in In a 10ml stoppered test tube, evaporate to dryness in a water bath, cool to room temperature, add 0.2ml of 5% vanillin glacial acetic acid solution, 0.8ml of perchloric acid, develop color in a 70°C water bath for 15 minutes, let cool...
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