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A batch ultrasonic reaction device
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A reaction device, ultrasonic technology, applied in the field of intermittent ultrasonic reaction device, can solve the problems of insufficient droplet refinement, low reliability, affecting three-phase reaction and mass transfer efficiency, etc.
Inactive Publication Date: 2017-04-19
HANGZHOU DIANZI UNIV
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Although devices such as fixed beds, fluidized beds, and high-gravity equipment have been widely used, especially high-gravity equipment creates a stable and adjustable centrifugal force field by rotating the liquid. It is stretched into a thin film and fine silk under the impact, resulting in a larger contact area between phases, which improves the transmission speed, and makes the relative speed of the gas-liquid two-phase in the chemical unit operation of the equipment such as rectification, absorption and complex reaction Greatly improved, but the device still has complex structure, high energy consumption, reliability is not as good as the general tower equipment, especially the insufficient droplet refinement and unstable refinement, which affect the three-phase reaction and mass transfer efficiency and other problems
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[0022] Such as figure 1 As shown, the present invention is an intermittent ultrasonic reaction device, including a protective cover 1, an ultrasonic acoustic system 2, a screw 3, a first throttle valve 4, an ultrasonic emission tank 5, a first bolt 6, a four-way shunt pipe 7, Pressure nozzle 8, flow guide hole 9, first fastening nut 10, gas-liquid exchange reaction chamber 12, second bolt 14, lead screw 15, third bolt 16, cover 17, second fastening nut 18, support ring 19 , double nuts 21, the second throttle valve 22, the third throttle valve 24, the fourth throttle valve 25, the fifth throttle valve 26, the booster pump 27, the stirring paddle 28 and the circulating liquid storage tank 29.
[0023] Such as figure 2 , image 3 , Figure 4 As shown, a 15 kHz ultrasonic acoustic system 2 is arranged at the center of the bottom of the ultrasonic emitting tank 5, and four 20 kHz ultrasonic acoustic systems 2 are symmetrically arranged around it. The protective cover 1 is ins...
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Abstract
The invention discloses an intermittent ultrasonic reaction device. The intermittent ultrasonic reaction device comprises a protective cover, ultrasonic acoustical systems, a screw, a first throttle valve, an ultrasonic transmitting groove, first bolts, a four-way flow dividing pipe, pressure nozzles, first clamp nuts, a gas-liquid exchange reaction chamber, gas guide holes, second bolts, lead screws, third bolts, a cover, second clamp nuts, a supporting ring, double nuts, a second throttle valve, a third throttle valve, a fourth throttle valve, a fifth throttle valve, a booster pump, stirring paddles and a circulation liquid storage groove. According to the intermittent ultrasonic reaction device, under the action of ultrasonic cavatition, reaction liquid is refined more evenly and finely; in the crystallization process, crystal grains can be effectively refined, and the crystal grains can be prevented from growing up; the catalyst surface can be updated in time, and the catalyst activity can be kept; the device can be widely used in the large-scale process such as sewage treatment and chemical industry production.
Description
technical field [0001] The invention relates to a novel intermittent ultrasonic reaction device, in particular to an intermittent ultrasonic reaction device. Background technique [0002] Nowadays, in the process of industrial production, with the continuous improvement of the requirements for safety, efficiency, and cleanliness, some process strengthening technologies and equipment have attracted more and more attention. The three-phase system of gas, liquid and solid is the most common system in chemical industry. Effectively improving the efficiency of mass transfer and heat transfer is always a problem that needs to be solved in this system. Although devices such as fixed beds, fluidized beds, and high-gravity equipment have been widely used, especially high-gravity equipment creates a stable and adjustable centrifugal force field by rotating the liquid. It is stretched into a thin film and fine silk under the impact, resulting in a larger contact area between phases, w...
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Application Information
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