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A kind of ink-jet printing pigment ink with high color fastness and preparation method thereof

An inkjet printing and pigment ink technology, which is applied to high color fastness inkjet printing pigment ink and its preparation, high color fastness inkjet printing pigment ink and its preparation field, can solve the problems of unsatisfactory color fastness and the like , to achieve the effect of improving dry rubbing printing fastness, improving hand feel, and improving rubbing fastness

Active Publication Date: 2016-08-10
JIANGSU GEMEIGAO DEV CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

U.S. Patent No. 7,338,988 and U.S. Pat. No. 7,030,1175 disclose a kind of preparation method in water-based pigment ink-jet ink, by adding polyacrylate emulsion in water-based pigment, and then improve the color fastness of plastic materials such as PE, PVC, PU, ​​but this ink is in The color fastness of printing on textiles is not ideal

Method used

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Examples

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Effect test

preparation example Construction

[0030] The preparation method for preparing the above-mentioned high color fastness inkjet printing pigment ink comprises the following steps:

[0031] For the preparation of ultra-fine coated pigments, first dissolve the polymerizable dispersant of the above ratio in the water of the above ratio, then put in the pH regulator, adjust the pH to 7~9, and then stir at 500~1200 rpm Add the pigment in the above ratio, stir evenly, transfer it to a sand mill, and grind it at a speed of 1600~2500 rpm for 1~5h to obtain an ultrafine pigment; then add the monomer in the above ratio dropwise, and continue grinding for 0.5 ~2h, take it out, transfer it to a four-necked flask equipped with a stirrer, a thermometer, and a condenser, feed in nitrogen, stir, raise the temperature to 60~90°C, slowly add the water-soluble initiator in the above ratio dropwise, and react for 0.5~10 After one hour, the reaction solution was taken out and filtered with a filter paper with a pore size of 500 nm to...

Embodiment 1

[0035] Dissolve 5.5g of allyloxynonylphenoxypropanol polyoxyethylene ammonium sulfate into 78.295g of water, add 0.2g of triethanolamine, and add 15g of carbon black pigment to the system at a stirring speed of 600 rpm , after stirring evenly, transfer it to a sand mill and grind it at a speed of 1600 rpm for 1.5 hours to obtain ultrafine carbon black, then add 1.00g of hydroxyethyl acrylate dropwise, continue grinding for 0.5 hours, take it out and transfer it to a machine equipped with a stirrer , thermometer, and condenser, feed nitrogen into the reactor, stir, heat up to 65°C, slowly add 0.005g ammonium persulfate dropwise, and react for 2.0 hours, take out the reaction solution, and filter it with filter paper with a pore size of 500nm to obtain ultrafine Coated carbon black pigment paste.

[0036] Weigh 40g of superfine coated pigment paste, then add 4g of ethylene glycol, 6g of isopropanol, 10g of glycerin, 2g of water-based polyurethane, 0.3g of Tween80, 0.1g of AFE-75...

Embodiment 2

[0038] Dissolve 6g of allyloxy hydroxypropyl sodium sulfonate into 71.695g of water, add 0.3g of sodium carbonate, and add 20g of C.I. Pigment Yellow 13 to the system at a stirring speed of 750 rpm, stir well and transfer to a sand mill Grind in the machine at a speed of 1800 rpm for 2 hours to obtain ultra-fine C.I. Pigment Yellow 13, then add 2g of propylene glycol diacrylate dropwise, continue grinding for 1 hour, take it out and transfer it to a reaction chamber equipped with a stirrer, a thermometer and a condenser Into the container, feed nitrogen, stir, heat up to 70°C, slowly add 0.005g of potassium persulfate dropwise, after 4.0 hours of reaction, take out the reaction solution, filter with filter paper with a pore size of 500nm, and obtain ultra-fine coated C.I. Pigment Yellow 13 colors pulp.

[0039] Weigh 30g ultra-fine coated C.I. Pigment Yellow 13, then add 5g of 1,3-propanediol, 10g of 1,4-butanediol, 15g of triethylene glycol, 5g of butane tetracarboxylic acid,...

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Abstract

The invention discloses an ink-jet printing pigment ink with high color fastness, which is characterized in that it comprises: ultrafine coated pigment paste, water-soluble co-solvent, crosslinking agent, surfactant, defoamer, bactericide, pH Conditioning agent, water; the ultrafine coated dye paste is composed of polymerizable dispersant, pH regulator, pigment, monomer and water-soluble initiator and water. The polymer is coated on the surface of the pigment particles by miniemulsion polymerization to improve the dispersion stability of the pigment particles and provide reactive groups that can be combined with the crosslinking agent. When coloring, the crosslinking agent and the pigment surface polymer together form a continuous, dense and smooth printing film on the surface of the fabric, thereby improving the rubbing fastness of the inkjet printing ink and improving the feel of the printed fabric to a certain extent.

Description

technical field [0001] The invention relates to a high color fastness inkjet printing pigment ink and a preparation method thereof, in particular to a high color fastness inkjet printing pigment ink and a preparation method thereof, belonging to the field of fine chemical science and technology. technical background [0002] Inkjet printing is a new type of textile printing technology recognized by the industry. This technology abandons the complicated process of plate making in traditional printing, greatly improves the printing accuracy, and realizes small batches, multiple varieties, multiple colors and personalized printing. Broad development prospects. Ink is an important consumable in digital printing production, and its research and development is a key step in promoting the development of digital inkjet printing technology. At present, the textile inkjet printing inks on the market are mainly dye inks, but due to the lack of versatility of dye inks, the printing pro...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D11/322C09D11/324C09D11/38D06P1/44D06P5/30D06P1/52D06P1/651C08F283/06C08F220/28C08F216/14C08F222/14C08F220/38C08F212/08C08F2/24C08F2/44
Inventor 王玉丰付少海陆建辉
Owner JIANGSU GEMEIGAO DEV CO LTD
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