High-thermal-conductivity elastic composite material and preparation method thereof
An elastic composite material and high thermal conductivity technology, applied in the field of composite materials, can solve the problems of limiting the application of pure polymers and low thermal conductivity, and achieve the effects of improving corrosion resistance, high thermal conductivity, and high thermal conductivity
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Embodiment 1
[0037] An embodiment of the present invention provides a high thermal conductivity elastic composite material, the high thermal conductivity elastic composite material includes curable silicone resin and composite thermal conductive filler, the composite thermal conductive filler is uniformly dispersed in the curable silicone resin, the curable The weight percentage of the silicone resin is 20%-60%, and the weight percentage of the composite heat-conducting filler is 40%-80%. The high thermal conductivity elastic composite material has the advantages of simple process, short production cycle, small product density, good elasticity, excellent corrosion resistance and high temperature resistance of the product.
[0038] Wherein, the curable silicone resin includes addition curable silicone resin, such as methyl vinyl silicone rubber with a molecular weight of 400,000-600,000.
[0039] Wherein, the composite heat-conducting filler includes any one of carbon nanotubes and graphene...
Embodiment 2
[0041] An embodiment of the present invention provides a method for preparing a high thermal conductivity elastic composite material. The preparation method includes: uniformly kneading the curable silicone resin, composite thermal conductivity filler and vulcanizing agent on a machine, wherein the machine can be a mixer Or a kneader; wherein, the curable silicone resin accounts for 20% to 60% of the total weight of the curable silicone resin and the composite thermally conductive filler, and the composite thermally conductive filler accounts for 40% of the total weight of the curable silicone resin and the composite thermally conductive filler. ~80%, the weight percentage of the vulcanizing agent and the curable silicone resin is 1:100~2:100, the vulcanizing agent can be 2,5-dimethyl-2,5-di-tert-butyl peroxy Hexane;
[0042] Vulcanize the homogeneously mixed mixture for 3 to 15 minutes at an air pressure of 100 to 300 MPa and a temperature of 160 to 180°C to obtain a high the...
Embodiment 3
[0044] Such as figure 1 and figure 2 The composite thermally conductive filler shown is the one involved in Example 2. The embodiment of the present invention provides a method for preparing a composite thermally conductive filler. The composite thermally conductive filler includes carbon nanotubes and 0.1-100 micron thermally conductive Powder, the preparation method of the composite thermally conductive filler comprises:
[0045] Disperse 20g of the heat-conducting powder into 100ml of an aqueous solution with a concentration of 1Mol / L cobalt nitrate to obtain a first mixed solution, and heat the first mixed solution to 70-90°C after ultrasonic treatment in an ultrasonic oscillator. During the process, the first mixed solution is mechanically stirred, and then ammonia water is added dropwise to the first mixed solution to obtain a second mixed solution until the pH value of the second mixed solution is greater than or equal to 12, and the second mixed solution is The mixe...
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