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A kind of colored yarn of creep-resistant polyester and its preparation method

A creep-resistant, polyester technology, applied in the direction of single-component copolyester rayon, bundle of newly extruded filaments, conjugated synthetic polymer rayon, etc., to improve hydrolysis resistance and expand application range, the effect of increasing the relative molecular mass

Active Publication Date: 2015-08-05
JIANGSU HENGLI CHEM FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are few studies on creep resistance of polyester fibers

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • A kind of colored yarn of creep-resistant polyester and its preparation method
  • A kind of colored yarn of creep-resistant polyester and its preparation method
  • A kind of colored yarn of creep-resistant polyester and its preparation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0054] Preparation of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol diglycidyl ether:

[0055] In a nitrogen atmosphere, mix epichlorohydrin and 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylidene]diphenol at a molar ratio of 4:1 , add 1.5% of 15mol / L sodium hydroxide solution of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl) ethylene] diphenol mass, at room temperature Stir the reaction for 16 hours; then cool to room temperature, then add 5mol / L of 30% of the mass of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol Sodium hydroxide solution, the sodium hydroxide solution is a solution saturated with anhydrous sodium carbonate, stirred and reacted at room temperature for 10 h; then extracted with chloroform, and the resulting organic phase was obtained by distilling off chloroform and excess epichlorohydrin to obtain a thick like liquid, which was added to absolute ethanol for recrystallization to obtain 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]dip...

Embodiment 2

[0064] Preparation of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol diglycidyl ether:

[0065] In a nitrogen atmosphere, mix epichlorohydrin and 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylidene]diphenol at a molar ratio of 4:1 , add 2.0% 10mol / L sodium hydroxide solution of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol mass, at room temperature Stir the reaction for 18 hours; cool to room temperature, then add 40% of the mass of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol of 3mol / L Sodium hydroxide solution, sodium hydroxide solution is a solution saturated with anhydrous sodium carbonate, stirred and reacted at room temperature for 15 hours; then extracted with chloroform, and the resulting organic phase was obtained by distilling off chloroform and excess epichlorohydrin to obtain a thick liquid, add it to absolute ethanol for recrystallization, and obtain 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol diglycidyl Crys...

Embodiment 3

[0074] Preparation of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol diglycidyl ether:

[0075] In a nitrogen atmosphere, mix epichlorohydrin and 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylidene]diphenol at a molar ratio of 4:1 , add 1.8% of 12mol / L sodium hydroxide solution of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol mass, at room temperature Stir the reaction for 17h; cool to room temperature, then add 35% of the mass of 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol of 4mol / L Sodium hydroxide solution, sodium hydroxide solution is a solution saturated with anhydrous sodium carbonate, stirred and reacted at room temperature for 13h; then extracted with chloroform, and the resulting organic phase was obtained by distilling off chloroform and excess epichlorohydrin to obtain a thick liquid, add it to absolute ethanol for recrystallization, and obtain 4,4'-[2,2,2-trifluoro-1-(trifluoromethyl)ethylene]diphenol diglycidyl Crystals of...

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Abstract

The invention relates to a creep-resistant polyester color yarn and its preparation method. The preparation method includes preparation of a creep-resistant polyester hyperviscous slice and preparation of a creep-resistant polyester color yarn. According to the preparation method, polyester is tackified through solid phase polycondensation and then the tackified polyester is mixed with a fluorine-containing epoxy compound to react so as to obtain the creep-resistant polyester hyperviscous slice; and the creep-resistant polyester color yarn is prepared from the obtained creep-resistant polyester hyperviscous slice by metering, mixing with a black masterbatch, extrusion, cooling, oiling, stretching and coiling. The creep-resistant polyester color yarn has a certain creep resistance, hydrolysis resistance and performance stability, can be used in a hot and humid environment for a long time, and has a huge prospect in the fields of automobile safety belts, bags fabric for military use, lifting belts and the like.

Description

technical field [0001] The invention relates to a colored yarn of creep-resistant polyester and a preparation method thereof, in particular to a colored yarn of creep-resistant polyester modified by using a fluorine-containing epoxy compound as an end-capping agent and a preparation method thereof. Background technique [0002] Polyester (PET) is one of the most widely used synthetic polymers by humans. It has high strength, high modulus and good heat resistance. It is the earliest linear thermoplastic polymer to achieve industrial applications. It is used in plastic packaging, film And chemical fiber and other fields have been widely used. Colored polyester fiber can be obtained by adding colorant before polyester spinning, which is called colored polyester yarn. The colorants used are generally high-temperature-resistant pigments with good biocompatibility, and can be completely wrapped in the fibers after presentation, and the pigment utilization rate is high. Polyester...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F6/84D01F8/14C08G81/00D01D5/08D01D5/088D01D5/096D01D7/00
Inventor 王丽丽汤方明尹立新杨大矛张元华
Owner JIANGSU HENGLI CHEM FIBER
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