Embedded capacitor material as well as preparation method and application thereof
A one-sided, ceramic filler technology, applied in the direction of circuit substrate materials, chemical instruments and methods, anodic oxidation, etc., can solve problems such as difficulty and troublesome implementation, and achieve improved dielectric strength, increased dielectric constant, and excellent dielectric strength Effect
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Embodiment 1
[0050] Dissolve 45g polyphenylene ether resin (hydroxyl equivalent weight 790), 55g brominated epoxy resin (epoxy resin B) and 20g phenoxy resin (C) in ethylene glycol methyl ether, and add 0.7 o-cresol novolak resin and 2-MI (2-methylimidazole) in molar ratio, and then mixed at room temperature to obtain glue. The obtained glue solution was coated on the release film, and then baked in an oven at 155°C for 5 minutes to cure to stage B, separated from the release film, and made into a thin film with a thickness of 5 μm.
[0051] Soak a 30-micron-thick aluminum sheet of type L3 in 10% sodium hydroxide solution for 20 minutes, take it out and rinse it with deionized water, then put it into an electrolytic cell containing 3% to 5% oxalic acid aqueous solution, and use the aluminum sheet As the anode and the copper plate as the cathode, the DC current density is 20A / dm 2 , with a voltage of 30V and a temperature of 40°C. After treatment for 10 minutes, take it out and rinse it wi...
Embodiment 2
[0054] Dissolve 45g polyphenylene ether resin (hydroxyl equivalent weight 790), 55g brominated epoxy resin (epoxy resin B) and 20g phenoxy resin (C) in ethylene glycol methyl ether, and add 0.7 o-cresol novolac resin and 2-MI (2-methylimidazole) in molar ratio, then add 90.5g of barium titanate with a median particle size of 10nm, and the volume percentage of barium titanate is 15%, then in Mix at room temperature to obtain a glue solution. The obtained glue solution was coated on the release film, and then baked in an oven at 155°C for 5 minutes to cure to stage B, separated from the release film, and made into a thin film with a thickness of 25 μm.
[0055] Soak a 70-micron-thick aluminum sheet in 10% sodium hydroxide solution for 20 minutes, take it out and rinse it with deionized water, then put it into an electrolytic cell containing 8% to 12% oxalic acid aqueous solution, and use the aluminum sheet as an anode , with a copper plate as the cathode, the DC current density...
Embodiment 3
[0058] Dissolve 45g of bisphenol A type epoxy resin (epoxy resin A), 55g of brominated epoxy resin (epoxy resin B) and 20g of phenoxy resin (C) in ethylene glycol methyl ether, and add relative O-cresol novolak resin and 2-MI (2-methylimidazole) with a 0.9 molar ratio of epoxy resin, and then add 342 g of barium titanate with a median particle diameter of 500 nm, and the volume percentage of barium titanate is 40%, and then mixed at room temperature to obtain a glue solution. The obtained glue solution was coated on the release film, and then baked in an oven at 155°C for 5 minutes to cure to stage B, separated from the release film, and made into a film with a thickness of 35 μm.
[0059] Soak a 100-micron-thick aluminum sheet in 10% sodium hydroxide solution for 20 minutes, take it out and rinse it with deionized water, then put it into an electrolytic cell containing 8% to 12% oxalic acid aqueous solution, and use the aluminum sheet as an anode , with a copper plate as the...
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