Water-based two-component fluorosilicone acrylic anticorrosive paint and preparation method thereof
A technology of fluorosilicone acrylic polyurethane and hydroxyfluorosilicone acrylic acid is applied in the field of waterborne two-component polyurethane anti-corrosion coating and its preparation, and can solve the problems of low solid content, low cross-linking density, environmental pollution, etc.
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Embodiment 1
[0079] A. Preparation of water-based hydroxyfluorosilicone acrylic resin:
[0080] a. Nuclear raw materials:
[0081]
[0082] Among them, the nuclear pre-emulsion emulsion includes:
[0083]
[0084] b. Shell raw materials:
[0085]
[0086] Preparation:
[0087] The first step: mixing the raw materials of the nuclear pre-emulsified emulsion to prepare the nuclear pre-emulsified emulsion;
[0088] Step 2: Add deionized water, emulsifier, buffer, and initiator in the raw materials of the nuclear part into the reactor, add 1.5 g of nuclear pre-emulsified emulsion under the stirring condition of 80 rpm, and react at a constant temperature of 80-85 °C for 15 minutes to form Seed emulsion, then add the remaining 33.5 g of nuclear pre-emulsified emulsion dropwise, the dropping time is 2-3 hours, the temperature is 80-85 °C, after the addition of nuclear pre-emulsified emulsion, 80-87 °C constant temperature reaction for 1-1.5 hours, Prepare a nuclear partial em...
Embodiment 2
[0097] A. Preparation of water-based hydroxyfluorosilicone acrylic resin:
[0098] Same as Example 1
[0099] B. Preparation of water-based two-component fluorosilicone acrylic polyurethane anticorrosion coating:
[0100]
[0101] The preparation steps of waterborne two-component fluorosilicone acrylic polyurethane anticorrosion coating are as follows:
[0102] Add deionized water, other additives except thickening and leveling agent into the stirring tank, add rutile titanium dioxide, ultra-fine mica powder, ultra-fine talc powder and precipitated barium sulfate under stirring, and disperse at a high speed of 900-1400rpm for 30 minutes , and then ground to a fineness of not more than 30 μm, then transported to the paint tank, adding water-based hydroxyfluorosilicone acrylic resin and thickening and leveling agent under the stirring condition of 80-90rpm, stirring evenly, discharging, filtering, and making into a finished product Membrane material composition;
[0103...
Embodiment 3
[0106] A. Preparation of water-based hydroxyfluorosilicone acrylic resin:
[0107] Same as Example 1
[0108] B. Preparation of water-based two-component fluorosilicone acrylic polyurethane anticorrosion coating:
[0109]
[0110] The preparation steps of waterborne two-component fluorosilicone acrylic polyurethane anticorrosion coating are as follows:
[0111] Add deionized water, other additives except thickening and leveling agent into the stirring tank, add rutile titanium dioxide, ultra-fine mica powder, ultra-fine talc powder and precipitated barium sulfate under stirring, and disperse at a high speed of 900-1400rpm for 30 minutes , and then ground to a fineness of not more than 30 μm, then transported to the paint tank, adding water-based hydroxyfluorosilicone acrylic resin and thickening and leveling agent under the stirring condition of 80-90rpm, stirring evenly, discharging, filtering, and making into a finished product Membrane material composition;
[01...
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