Novel preparation method for noble composite metallic bond composite wire materials
A technology of noble metal and composite bonding, which is applied in the field of noble metal composite bonding wire for semiconductor packaging, to achieve uniform thickness
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Embodiment 1
[0032] Preparation of Ag / Cu Composite Wire
[0033] Preparation:
[0034] (1) Ag with a purity greater than 99.999% is selected to form a round tube through ingot casting, extrusion, and drawing. The outer diameter of the round tube is 20 mm, the wall thickness is 2 mm, and the length is 100 mm.
[0035] (2) Wipe and clean the inner wall of the Ag tube with acetone.
[0036] (3) The Ag tube is placed in a water-cooled mold with an inner diameter of 20mm.
[0037] (4) Place the water-cooled mold in a vacuum furnace, and pass cooling water, the water intake is 10L / min, the water pressure is 0.5MPa, and the water temperature is ≤20°C. Cu with a purity ≥ 99.95% is placed in a vacuum induction melting furnace, and the casting position is adjusted.
[0038] (5) Pre-vacuumize and fill with argon for repeated cleaning twice, and evacuate to a high vacuum of 6×10 -3 Pa, and then filled with argon up to 0.05Mpa, heating and melting.
[0039] (6) Casting: The molten metal of the cor...
Embodiment 2
[0049] Preparation of Au / Ag Composite Wire
[0050] Preparation:
[0051] (1) Au with a purity greater than 99.999% is selected to form a round tube through ingot casting, extrusion, and drawing. The outer diameter of the round tube is 18 mm, the wall thickness is 1.5 mm, and the length is 100 mm.
[0052] (2) Wipe and clean the inner wall of the Au tube with acetone.
[0053] (3) The Au tube is placed in a water-cooled mold with an inner diameter of 18 mm.
[0054] (4) Put the water-cooled mold in the vacuum furnace, and pass cooling water, the water intake is 15L / min, the water pressure is 0.5MPa, and the water temperature is ≤20°C. Ag with a purity of ≥99.99% is placed in a vacuum induction melting furnace, and the casting position is adjusted.
[0055] (5) Pre-vacuumize and fill with argon for repeated cleaning twice, and evacuate to a high vacuum of 6×10 -3 Pa, and then filled with argon up to 0.05Mpa, heating and melting.
[0056] (6) Casting: pour the molten metal ...
Embodiment 3
[0066] Preparation of Pd / Cu Composite Wire
[0067] Preparation:
[0068] (1) Select Pd with a purity greater than 99.999% to form a round tube through ingot casting, extrusion, and drawing. The outer diameter of the round tube is 15 mm, the wall thickness is 1.5 mm, and the length is 100 mm.
[0069] (2) Wipe and clean the inner wall of the Pd tube with gasoline.
[0070] (3) The Pd tube is placed in a water-cooled mold with an inner diameter of 15mm.
[0071] (4) Put the water-cooled mold in the vacuum furnace, and pass the cooling water, the water intake is 8L / min, the water pressure is 0.4MPa, and the water temperature is ≤20°C. Cu with a purity ≥ 99.99% is placed in a vacuum induction melting furnace, and the casting position is adjusted.
[0072] (5) Pre-vacuumize and fill with argon for repeated cleaning twice, and evacuate to a high vacuum of 6×10 -3 Pa, then filled with argon to reach 0.05Mpa, and heated up for melting.
[0073] (6) Casting: Pour the molten metal o...
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