SCR (selective catalytic reduction) flue gas denitration catalyst regeneration method
A denitration catalyst and catalyst technology, which can be used in catalyst regeneration/reactivation, chemical instruments and methods, physical/chemical process catalysts, etc., can solve problems such as serious pollution and environmental pollution, and achieve the effect of cheap promotion and use
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Embodiment 1
[0037] 1. Preparation of cleaning solution, weigh 0.05 Kg (0.01%) of TX-10 emulsifier, weigh 49.95 Kg (99.9%) of oxalic acid with an acid molar concentration of 1.5 mol / L, and perform ultrasonic treatment for 10 minutes to make it mix Evenly, it is prepared into 50 Kg cleaning solution.
[0038] 2. Preparation of active replenishing liquid
[0039] The first step: Weigh JFC type accelerator 0.05 Kg (0.1%), diffusion agent sodium dinaphthyl methane disulfonate 2.5Kg (5%), zirconium nitrate 2.5 Kg (5%), copper nitrate 2.5 Kg (5% ), deionized water 8 Kg (16%), stirring speed is 100 rev / min, mechanical stirring 120 minutes, make it mix homogeneously;
[0040] Step 2: Weigh 15 Kg (30%) of tetrabutyl titanate, 15 Kg (30%) of absolute ethanol, and 4.45 Kg (8.9%) of deionized water. Stirring speed is 1000 rev / min, mechanical stirring for 10 minutes to make it mix evenly;
[0041] Step 3: Add liquid A to liquid B, stir at a speed of 500 rpm, mechanically stir for 90 minutes, and pre...
Embodiment 2
[0055] 1. Preparation of cleaning solution, weigh 5 Kg (10%) of OP-10 emulsifier, weigh 45 Kg (90%) of nitric acid with an acid molar concentration of 3 mol / L, and perform ultrasonic treatment for 35 minutes to make it mix Evenly, prepare 50Kg cleaning solution.
[0056] 2. Preparation of active replenishing liquid
[0057] The first step: take by weighing JFC-1 type accelerator 5 Kg (10%), diffusion agent sodium dinaphthyl methane disulfonate 0.05 Kg (0.1%), nickel nitrate 2.5 Kg (5%), lanthanum nitrate 5 Kg ( 10%), molybdenum nitrate 5 Kg (10%), zirconium sulfate 5 Kg (10%), ferric nitrate 2.5 Kg (5%), deionized water 22 Kg (44%), stirring speed is 1000 rpm, mechanical Stir for 10 minutes to make it evenly mixed;
[0058] Step 2: Weigh 0.5 Kg (1%) of tetrabutyl titanate, 0.5 Kg (1%) of absolute ethanol, and 1.95 Kg (3.9%) of deionized water. The stirring speed is 100 rpm, and the mechanical stirring is carried out for 120 minutes to make it evenly mixed;
[0059] Step 3:...
Embodiment 3
[0070] 1. Preparation of cleaning solution, weigh 5 Kg (10%) of OP-10 emulsifier, weigh 45 Kg (90%) of sulfuric acid with an acid molar concentration of 0.018mol / L, and perform ultrasonic treatment for 60 minutes to mix Evenly, prepare 50Kg cleaning solution.
[0071] 2. Preparation of active replenishing liquid
[0072] The first step: weigh JFC-2 type accelerator 2.5 Kg (5%), diffusion agent sodium dinaphthyl methane disulfonate 5Kg (10%), molybdenum sulfate 5Kg (10%), copper sulfate 5Kg (10%) , cerium sulfate 2.5Kg (5%), deionized water 20Kg (40%), stirring speed is 500 revs / min, mechanical stirring 60 minutes, make it mix homogeneously;
[0073] Step 2: Weigh 2.5Kg (5%) of tetrabutyl titanate, 2.5Kg (5%) of absolute ethanol, and 5Kg (10%) of deionized water. Stirring speed is 1000 rpm, mechanical stirring for 60 minutes, mixing evenly;
[0074] Step 3: Add liquid A to liquid B, stir at a speed of 1000 rpm, mechanically stir for 60 minutes, and prepare 50kg of active rep...
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