A kind of rare earth permanent magnet and its preparation method
A rare earth permanent magnet and magnet technology, which is applied in the manufacture of magnetic objects, permanent magnets, inductors/transformers/magnets, etc., can solve the problems of magnet corrosion resistance, poor solubility of powder in water or organic solvents, uneven distribution, etc. Achieve the effect of improving coercivity, improving uniformity and reducing residues
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Embodiment 1-2
[0037] Smelt the alloy to get (Nd, Pr) a Dy b Fe (1-a-b-c) B c (a = 14.5, b = 0.6, c = 5.8, a, b, and c are atomic percentages), the ingot alloy is coarsely crushed and hydrogen crushed according to the conventional method, jet milled into fine powder, and then mixed Uniform, then oriented by a 2.0T magnetic field and pressed into shape, subjected to 180MPa isostatic pressing, and the green body was sintered at 1070°C for 3 hours to obtain a rough magnet, and the sintered rough magnet was cut into small square pieces of 12mm×12mm×2mm for processing magnet. Divided into A (original sample), B (comparative example), C (example 1), D (example 2) four groups of 100 pieces each. The two groups of samples A and B are comparative samples, in which the samples of group A are not treated, and the samples of group B are pickled with a mass ratio of 3% nitric acid aqueous solution, and then DyF is arranged on the surface of the samples. 3 , Dy 2 o 3 and DyOF powder (the mass perce...
Embodiment 3
[0048] Smelting the alloy by strip technology to obtain (Nd, Pr, Sc) a Dy b co d Fe (1-a-b-c-d) B c (a=15, b=0.6, c=5.8, d=1.0, a, b, c, and d are atomic percentages), the flakes are subjected to hydrogen crushing and air-jet milling in a conventional manner to make fine powder , and then mixed evenly, and then oriented by a 2.0T magnetic field and pressed into shape, subjected to 180MPa isostatic pressing, and the green body was sintered at 1060°C for 3 hours to obtain a rough magnet, and the sintered rough magnet was cut into small square pieces of 12mm×12mm×2mm As a belt handle magnet. The magnet to be treated carries out routine pickling through the nitric acid aqueous solution of 4% mass ratio, then arranges the fluoride powder of R2 on its surface, the nitrate powder of R3 and the phosphate powder of R4, R2 is Dy and Y (Dy, Y mass ratio 3: 1), R3 is Tb, R4 is Tb, three powder mass percentages are respectively 73%, 12%, 15%, and the average particle size is respectiv...
Embodiment 4
[0050] The alloy is smelted by strip strip technology to obtain Nd a Dy b Fe (1-a-b-c-d) Al d B c (a=15, b=0.3, c=6.0, d=0.3, a, b, c, d are atomic percentages) of flakes, the flakes are subjected to hydrogen crushing and jet milling in a conventional manner to make fine powder , and then mixed evenly, and then oriented by a 2.0T magnetic field and pressed into shape. After 180MPa isostatic pressing, the green body was sintered at 1060°C for 3.5h, and then aged at 450°C for 3.5h to obtain a rough magnet. The aged blank was cut into A small square piece of 12mm×12mm×3mm is used as the magnet to be processed. The magnet to be treated carries out conventional alkali washing through 2% mass ratio of sodium silicate aqueous solution, then arranges the fluoride powder of R2 on its surface, the nitrate powder of R3 and the phosphate powder of R4, R2 is Tb and Sc (Tb and Sc The mass ratio is 4:1), R3 is Dy and Ho (the mass ratio of Dy and Ho is 4:1), R4 is Dy and Er (the mass rat...
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