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Method for preparing TiC and TiB hybrid reinforced Ti-Al-Sn-Zr-Mo-Si-based composite board

A composite material and sheet technology, which is applied in the field of preparation of reinforced Ti-Al-Sn-Zr-Mo-Si matrix composite material sheets, can solve problems such as the decrease of tensile properties, and achieve the effect of excellent mechanical properties

Inactive Publication Date: 2012-01-04
HARBIN INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The present invention is to solve the technical problem that the tensile properties of the existing iC particle reinforced Ti-Al-Sn-Zr-Mo-Si high-temperature titanium alloy composite sheet material drop sharply above 650°C, and provide TiC and TiB hybrid reinforced Ti -Preparation method of Al-Sn-Zr-Mo-Si matrix composite material plate

Method used

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  • Method for preparing TiC and TiB hybrid reinforced Ti-Al-Sn-Zr-Mo-Si-based composite board
  • Method for preparing TiC and TiB hybrid reinforced Ti-Al-Sn-Zr-Mo-Si-based composite board

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specific Embodiment approach 1

[0010] Embodiment 1: The preparation method of the TiC and TiB hybrid reinforced Ti-Al-Sn-Zr-Mo-Si-based composite material plate of this embodiment is carried out according to the following steps: 1. Reinforce Ti-Al-Sn by TiC and TiB hybrid - The volume percentage of TiC particles in the Zr-Mo-Si based composite material plate is 0.5% to 12.5%, the volume percentage of TiB particles is 0.5% to 12.5%, and the volume percentage of Ti-Al-Sn-Zr-Mo-Si titanium alloy The percentage is 75% to 99%, and the titanium powder, graphite powder, titanium diboride powder and raw materials for preparing Ti-Al-Sn-Zr-Mo-Si titanium alloy are respectively weighed, and the molar ratio of titanium powder to graphite powder is 2~6:1, the molar ratio of titanium powder and titanium diboride powder is 2~6:1; 2. Add the titanium powder, graphite powder and titanium diboride powder weighed in step 1 into the mixer Mix evenly, and then use a cold isostatic press to keep the mixed powder at a pressure o...

specific Embodiment approach 2

[0011] Embodiment 2: The difference between this embodiment and Embodiment 1 is that the fineness of the titanium powder described in step 1 is 300 mesh to 350 mesh, the fineness of graphite powder is 2 μm to 5 μm, and the titanium diboride powder The fineness is 2μm~5μm. Other steps and parameters are the same as in the first embodiment.

specific Embodiment approach 3

[0012] Specific embodiment three: the difference between this embodiment and specific embodiment one or two is that the fineness of the titanium powder described in step one is 325 mesh, the fineness of graphite powder is 3.5 μm, and the fineness of titanium diboride powder is 3 μm. Other steps and parameters are the same as those in Embodiment 1 or 2.

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Abstract

The invention relates to a method for preparing a TiC and TiB hybrid reinforced Ti-Al-Sn-Zr-Mo-Si-based composite board, and relates to a method for preparing a titanium-based composite board. By the method, the problem that the tensile property of the conventional TiC granule reinforced Ti-Al-Sn-Zr-Mo-Si-based composite board is reduced drastically at the temperature of more than 650 DEG C. The method comprises the following steps of: calculating required titanium power, titanium diboride, graphite powder and other materials according to the volume percentage of TiC, TiB and Ti-Al-Sn-Zr-Mo-Si-based titanium alloys in the composite board; preparing a precast block by using the titanium power, the titanium diboride and the graphite powder, smelting the precast block together with other materials, and thus obtaining a cast ingot; and forging, rolling, performing heat treatment, and thus obtaining the composite board, wherein the tensile strength of the composite board is between 810 and 890MPa at the temperature of 650 DEG C, so the composite board can be used in the field of aerospace.

Description

technical field [0001] The invention relates to a method for preparing reinforced Ti-Al-Sn-Zr-Mo-Si matrix composite material plate. Background technique [0002] With the rapid development of aerospace technology and the automobile industry, the flight distance and flight speed of various new aircraft have increased, and higher and higher requirements have been put forward for lightweight, high-strength, heat-resistant materials and their precision thermoforming technology. Due to the many outstanding advantages of particle-reinforced titanium-based composites, such as: low density, high specific strength and specific elastic modulus, it can still maintain high enough strength and stiffness at high temperatures, etc., which makes it suitable for aerospace, aviation and Very competitive material for heat-resistant structural profiles for automotive applications. At present, major developed countries in the world are actively carrying out research work on particle-reinforced...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C14/00C22C32/00C22C1/02C22F1/18
Inventor 陈玉勇孔凡涛张长江肖树龙徐丽娟
Owner HARBIN INST OF TECH
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