A kind of fine-grained WC-based cemented carbide material and preparation method thereof
A cemented carbide and fine-grained technology, which is applied in the field of cemented carbide, can solve the problems of micropore formation, poor product density, crystal deformation and agglomeration, etc., and achieve the effects of increased strength, short sintering time and high hardness
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[0032] Wherein, the preparation method of the fine-grained WC-based cemented carbide material of the present invention includes the following process steps and contents:
[0033] 1) Initial processing: Weigh the raw materials according to the composition, add the raw materials WC powder, binder powder, grain inhibitor powder and reinforcing agent weighed in proportion to the stirring ball mill tank for stirring, and the stirring time is preferably 5-10 hours ;
[0034] 2) Drying: In a vacuum drying oven, dry the slurry after initial processing, and the drying conditions are preferably at 80-100°C and a vacuum degree of 0-0.33Pa for 6-10 hours;
[0035] 3) Grinding: Grinding the dried powder to form a powder with a pore size below 1 mm;
[0036] 4) Loading: Put the ground powder into the sintering mold and compact it;
[0037] 5) Sintering: Sintering and molding are carried out in a sintering furnace, preferably in a medium frequency induction heating sintering furnace.
Embodiment 1
[0039] The manufacturing method and process flow of the fine-grained WC-based cemented carbide in the embodiment of the present invention are as follows:
[0040] 1) Initial processing: Weigh the raw materials according to the composition, and the raw materials are:
[0041] 0.9μm WC: 85%, Mo: 5%; TiC: 8%; Cr 3 C 2 : 1%; Si: C1%;
[0042] The raw materials weighed in proportion were added into the stirring ball mill tank for stirring, and the stirring time was 8 hours;
[0043] 2) Drying: In a vacuum drying oven, dry the pre-processed slurry for 8 hours under the drying conditions of 90°C and vacuum degree of -0.2Pa;
[0044] 3) Grinding: Grinding the dried powder to form a powder with a pore size below 1 mm;
[0045] 4) Loading: Put the ground powder into the sintering mold and compact it;
[0046] 5) Sintering: Sintering and molding are carried out in a sintering furnace, preferably in a medium frequency induction heating sintering furnace.
[0047] The data of the fin...
Embodiment 2
[0050] The manufacturing method and process flow of the fine-grained WC-based cemented carbide in the embodiment of the present invention are as follows:
[0051] 1) Initial processing: Weigh the raw materials according to the composition, and the raw materials are:
[0052] 1μm WC: 86%, Ni: 5%; VC: 7%; Cr 3 C 2 : 1%; Si: C1%;
[0053] The raw materials weighed in proportion were added into the stirring ball mill tank for stirring, and the stirring time was 8 hours;
[0054] 2) Drying: In a vacuum drying oven, dry the pre-processed slurry for 8 hours under the drying conditions of 90°C and vacuum degree of -0.2Pa;
[0055] 3) Grinding: Grinding the dried powder to form a powder with a pore size below 1 mm;
[0056] 4) Loading: Put the ground powder into the sintering mold and compact it;
[0057] 5) Sintering: Sintering and molding are carried out in a sintering furnace, preferably in a medium frequency induction heating sintering furnace.
[0058]The data of the fine-gr...
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