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Manufacturing method of isolation board for sintering

A manufacturing method and technology for isolating plates, which are applied in the field of plate blank sintering, can solve the problems of metal plate deformation, contact surface damage, and high thermal spraying process cost, and achieve the effects of preventing sintering adhesion, high production efficiency and simple process.

Active Publication Date: 2013-08-21
NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The contact surfaces of the stacked sheet blank products present a tight combination of the same material with a certain extrusion force. During the sintering process, mutual diffusion occurs between the contact surfaces of the sheet blanks, and it is easy to bond (weld) together, seriously The sintered plate blanks cannot be separated when the sintering temperature is not high; sometimes they can be separated when the sintering temperature is not high, but the contact surface is seriously damaged
In order to solve the above problems, the methods currently used are: ①Separation plate method, adding a layer of separation plate between the laminates, the plate requires higher temperature resistance (above the sintering temperature), and generally uses high-temperature ceramics that do not react with the sintered body Plate, ceramic cloth or ceramic paper, etc. This method can effectively prevent the plate-shaped sintered body from sticking, but the ceramic material will crack after several times of sintering, and the volatilization of the ceramic paper will cause pollution of the sintered material and damage the sintering process. The atmosphere of the furnace; ②Oxide sand bedding method, evenly spread fillers between layered sintered materials, the fillers are granular, generally oxide sand (alumina or zirconia), this method will cause concaves on the surface of the sintered body Pit, the use of fine alumina filler can avoid pits, but fine alumina sand is easy to fly when the vacuum furnace is started, pollute the furnace cavity, affect the vacuum degree, and affect the service life of the sintering furnace. Covering and Sealing and other measures are relatively cumbersome when using this method to install the furnace. Sometimes it is necessary to put the plate blank into the sintering furnace first, and then spread oxide sand on the plate blank; The surface of the plate blank (the plate must be resistant to sintering high temperature) is thermally sprayed with a layer of alumina (zirconium), which is very thin and firmly bonded. This method can achieve the effect of sintering isolation, but the cost of thermal spraying process is high. Moreover, the sprayed layer will fall off after 5-6 times of sintering, and the falling off part will not have the isolation effect. The spraying method will cause high temperature during the production process, and the thinner metal plate will be deformed. Using it as a separator will cause powder metallurgy plates. Deformation of the sintered body of the billet; although the deformation can be avoided by using a thicker metal plate, the lower sintered body will be too heavy and thinner when superimposed, or it will be too dense

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] (1) Slurry preparation: prepare polyvinyl alcohol into an aqueous solution with a mass percentage concentration of 2%, then add alumina powder (or zirconia powder) to the prepared aqueous solution, and stir evenly at 50°C to obtain a slurry , the amount of alumina powder (or zirconia powder) added is 50g per liter of aqueous solution;

[0017] (2) brush coating slurry: adopt the flat metal plate (stainless steel plate) of surface, evenly coat the slurry described in the step (1) on one side of the metal plate, make the slurry cover the surface of the metal plate completely during coating;

[0018] (3) Drying: putting the metal plate coated with the slurry in step (2) into an oven (the temperature is controlled between 80° C. and 110° C.) to dry to obtain a separator for sintering.

[0019] The isolation plate manufactured in this embodiment is an isolation plate that is in contact with the sintered plate blank on one side and functions as isolation between the bottom an...

Embodiment 2

[0021] (1) Slurry preparation: prepare polyvinyl alcohol into an aqueous solution with a concentration of 10% by mass, then add zirconia powder (or alumina powder) to the prepared aqueous solution, and stir evenly at 80°C to obtain a slurry , the amount of zirconia powder (or alumina powder) added is 100g per liter of aqueous solution;

[0022] (2) brush coating slurry: adopt the flat metal plate (stainless steel plate) of surface, evenly coat the slurry described in the step (1) on both sides of the metal plate, make the slurry cover the surface of the metal plate completely during coating;

[0023] (3) Drying: putting the metal plate coated with the slurry in step (2) into an oven (the temperature is controlled between 80° C. and 110° C.) to dry to obtain a separator for sintering.

[0024] The separator made in this embodiment is a separator whose two sides are in contact with the sintered blanks and serves as a separator between the sintered blanks during sintering. When ...

Embodiment 3

[0026] (1) Slurry preparation: prepare polyvinyl alcohol into an aqueous solution with a mass percent concentration of 6%, then add zirconia powder (or alumina powder) to the prepared aqueous solution, and stir evenly at 100°C to obtain a slurry , the total amount of zirconia powder (or aluminum oxide powder) added is 150g per liter of aqueous solution;

[0027] (2) brush coating slurry: adopt the flat metal plate (stainless steel plate) of surface, evenly coat the slurry described in the step (1) on one side of the metal plate, make the slurry cover the surface of the metal plate completely during coating;

[0028] (3) Drying: putting the metal plate coated with the slurry in step (2) into an oven (the temperature is controlled between 80° C. and 110° C.) to dry to obtain a separator for sintering.

[0029] The isolation plate manufactured in this embodiment is an isolation plate that is in contact with the sintered plate blank on one side and functions as isolation between t...

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PUM

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Abstract

The invention discloses a manufacturing method of an isolation board for sintering. The method comprises the following steps of: 1, preparing polyvinyl alcohol or cellulose into an aqueous solution, adding metal oxide powder and stirring uniformly to obtain slurry; 2, uniformly coating slurry on one or two faces of a metal board with a flat surface; and 3, putting the slurry-coated metal board into a drying oven for drying to obtain the isolation board for sintering. The manufacturing method has the advantages of simple procedures, low cost and high production efficiency. The manufactured isolation board for sintering can be used repeatedly. After the isolation board is used, organic matters are volatilized, oxide powder particles fall, and slurry can be repainted on the recycled metal board after soot cleaning, so that an isolation board for sintering is manufactured for repeated use. The isolation board for sintering manufactured with the method is taken as an isolation layer between laminated plate blanks, so that sintering adhesion of the plate blanks can be prevented effectively, the surfaces of the plate blanks are protected, and the surface quality of the sintering plate blanks is not influenced simultaneously.

Description

technical field [0001] The invention belongs to the technical field of plate blank sintering, and in particular relates to a method for making a sintering isolation plate. Background technique [0002] Sintering in a sintering furnace (or heat treatment furnace) is one of the important processes in material processing technology, especially for powder metallurgy materials. Sintering is an essential process to ensure the final properties of materials. For the sintering of powder metallurgy sheet blanks, layered stacking and sintering in a sintering furnace is a common method; and the heat treatment of a large number of metal sheet blanks can also be stacked and placed in a furnace for processing. The biggest advantage is high production efficiency and low cost. The contact surfaces of the stacked sheet blank products present a tight combination of the same material with a certain extrusion force. During the sintering process, mutual diffusion occurs between the contact surfa...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B05D7/16B05D7/24B05D3/02C09D129/04C09D101/02C09D7/12B22F3/10
Inventor 王建永汤慧萍朱纪磊敖庆波李程陈金妹葛渊支浩杨保军康新婷谈萍汪强兵李亚宁迟煜頔许忠国奚正平
Owner NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH
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