Method for preparing multifunctional titanium dioxide pigment with chlorination method
A titanium dioxide, multi-functional technology, applied in chemical instruments and methods, inorganic pigment treatment, fibrous fillers, etc., can solve problems such as insufficient weather resistance, prevent powder loss, improve dispersion performance, and improve weather resistance. Effect
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Embodiment 1
[0021] 1. Weigh 500g of the primary product of titanium dioxide by chloride method, and the content of alumina in the primary product is 1.2%.
[0022] 2. Add deionized water to prepare a 500g / l slurry, adjust the pH value of the slurry to 10.0 with sodium hydroxide solution, add sodium hexametaphosphate solution, the amount of sodium hexametaphosphate solution is based on five Phosphorus oxide accounted for 0.5% by weight of the primary product of titanium dioxide, and dispersed for 30 minutes.
[0023] 3. Add sand into the sand mill, and sand-mill the above-mentioned slurry. After sand-milling, the average particle size of the slurry is 300nm, and the particle size distribution is calculated by quantity. The proportion exceeding 1000nm is 0.24%.
[0024] 4. Remove the grinding media from the slurry.
[0025] 5. Raise the temperature of the above slurry to 80°C.
[0026] 6. Add sodium silicate solution at one time, the amount of sodium silicate solution added is 1.0% based ...
Embodiment 2
[0033] 1. Weigh 400g of the primary product of titanium dioxide by chloride method, and the content of alumina in the primary product is about 0.6%.
[0034] 2. Add deionized water to prepare a 400g / l slurry, adjust the pH value of the slurry to 9.0 with sodium hydroxide solution, add sodium hexametaphosphate solution, the amount of sodium hexametaphosphate solution is five Phosphorus oxide accounted for 0.1% by weight of the primary product of titanium dioxide, and dispersed for 20 minutes.
[0035] 3. Add sand into the sand mill, and sand-mill the above-mentioned slurry. The average particle size of the slurry is 365nm, and the particle size distribution is calculated by quantity, and the proportion exceeding 1000nm is 0.55%.
[0036] 4. Remove the grinding media from the slurry.
[0037] 5. Raise the temperature of the sand-milled slurry to 60°C.
[0038] 6. Add sodium silicate solution at one time, the amount of sodium silicate solution added is 0.5% based on the weight ...
Embodiment 3
[0045] 1. Weigh 600g of the primary product of titanium dioxide by the chloride method, and the content of alumina in the primary product is 1.5%.
[0046] 2. Add deionized water to prepare a 500g / l slurry, adjust the pH value of the slurry to 11.0 with sodium hydroxide solution, add sodium hexametaphosphate solution, the amount of sodium hexametaphosphate solution is based on five Phosphorus oxide accounts for 1.0% by weight of the primary titanium dioxide product, and is dispersed for 30 minutes.
[0047] 3. Add sand into the sand mill, and sand-mill the above-mentioned slurry. The average particle size of the slurry is 500nm, and the particle size distribution is calculated by quantity, and the proportion exceeding 1000nm is 1.0%.
[0048] 4. Remove abrasive impurities from the slurry.
[0049] 5. Raise the temperature of the sand-milled slurry to 90°C.
[0050] 6. Add 2.0% sodium silicate solution at one time, based on the weight of silicon dioxide in sodium silicate as ...
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