Composite material with high dielectric constant and preparation method thereof
A technology of high dielectric constant and composite material, applied in the field of materials, can solve the problems of high cost and complicated preparation process, and achieve the effect of low cost, large dielectric constant and low price
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Embodiment 1
[0034] A method for preparing a high dielectric constant composite material, characterized in that it comprises the following steps,
[0035] In the first step, barium titanate powder and copper powder are used as raw materials, according to BaTiO 3 / xCu, x=30wt.% carry out batching;
[0036] In the second step, the raw material, ball milling medium and ball stone are mixed, and then ball milled on a planetary ball mill for 4 hours in a resin ball mill tank, wherein the mass ratio of raw material, ball milling medium and ball stone is: raw material: ball milling medium: ball stone=1 :1:1.5;
[0037] The third step is to dry the ball-milled slurry in a vacuum oven at a temperature not higher than 50°C, then use PVA with a concentration of 3% to granulate, pass the granulated granules through a 150-mesh sieve, and stale for 24 hours;
[0038] The fourth step is to put the stale grains into a steel mold and press them into a cylindrical green body under a pressure of 5MPa, hold...
Embodiment 2
[0043] A method for preparing a high dielectric constant composite material, characterized in that it comprises the following steps,
[0044] In the first step, barium titanate powder and copper powder are used as raw materials, according to BaTiO 3 / xCu, x=10wt.% carry out batching;
[0045] In the second step, the raw material, ball milling medium and ball stone are mixed, and then ball milled on a planetary ball mill for 4 hours in a resin ball mill tank, wherein the mass ratio of raw material, ball milling medium and ball stone is: raw material: ball milling medium: ball stone=1 :1.2:2;
[0046] The third step is to dry the ball-milled slurry in a vacuum oven at a temperature not higher than 50°C, and then use PVA with a concentration of 4% to granulate, pass the granulated granules through a 150-mesh sieve, and stale for 24 hours;
[0047] The fourth step is to put the stale grains into a steel mold and press them into a cylindrical green body under a pressure of 5MPa, ...
Embodiment 3
[0052] A method for preparing a high dielectric constant composite material, characterized in that it comprises the following steps,
[0053] In the first step, barium titanate powder and copper powder are used as raw materials, according to BaTiO 3 / xCu, x=1wt.% for batching;
[0054] In the second step, raw materials, ball milling media and ball stones are mixed, and then ball milled on a planetary ball mill for 4 hours in a resin ball mill tank, wherein the mass ratio of raw materials, ball milling media and ball stones is: raw materials: ball milling media: ball stones=1.5 :1.5:2;
[0055] The third step is to dry the ball-milled slurry in a vacuum oven at a temperature not higher than 50°C, and then use PVA with a concentration of 5% to make granules. The granulated granules are passed through a 150-mesh sieve and aged for 24 hours;
[0056] The fourth step is to put the stale grains into a steel mold and press them into a cylindrical green body under a pressure of 5MPa...
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