Interior wall adornment leather and preparation method
A technology for decorative leather and interior walls, applied in textiles, papermaking, fiber treatment, etc., can solve problems such as poor flame retardancy, dirt resistance, and poor hand feeling
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Embodiment 1
[0045] This example is used to illustrate the interior wall decorative leather provided by the present invention and its preparation method.
[0046] 1. Preparation of slurry
[0047] 1-1PUD-2 slurry
[0048] (1) Add 60.02g of isophorone diisocyanate to 150g of poly-1,4-butylene adipate diol (Mn=2000) and react at 80°C for 120 minutes;
[0049] (2) Add 45g of acetone, control the temperature of the reaction system at 50°C, add 11.40g of dimethylolpropionic acid and 16.01g of tris(dipropylene glycol) phosphite, and react at 75°C for 180 minutes until the NCO value drops to 1.5% by weight;
[0050] (3) Control the temperature of the reaction system at 40° C., add 8.59 g of triethylamine for neutralization reaction for 30 minutes;
[0051] (4) adding the neutralized and hydrophilic prepolymer into 350g deionized water for high-speed emulsification and dispersion to obtain a water-based polyurethane dispersion with a solid content of 40%;
[0052] (5) Add 4.6g of thickener, 2....
Embodiment 2
[0079] This example is used to illustrate the interior wall decorative leather provided by the present invention and its preparation method.
[0080] 1. Preparation of slurry
[0081] 1-1PUD-2 slurry
[0082] (1) Add 60.02g of isophorone diisocyanate to 150g of poly-1,4-butylene adipate diol (Mn=2000) and react at 80°C for 120 minutes;
[0083] (2) Add 45g of acetone, control the temperature of the reaction system at 50°C, add 11.32g of dimethylolpropionic acid and 14.42g of N,N-bis(2-hydroxyethyl)aminomethylphosphonic acid diethyl ester, in React at 75°C for 180 minutes until the NCO value drops to 1.5% by weight;
[0084] (3) Control the temperature of the reaction system at 40° C., add 8.53 g of triethylamine for neutralization reaction for 30 minutes;
[0085] (4) adding the neutralized and hydrophilic prepolymer into 350g deionized water for high-speed emulsification and dispersion to obtain a water-based polyurethane dispersion with a solid content of 40%;
[0086] (...
Embodiment 3
[0113] This example is used to illustrate the interior wall decorative leather provided by the present invention and its preparation method.
[0114] 1. Preparation of slurry
[0115] 1-1PUD-2 slurry
[0116] (1) Add 60.02g of isophorone diisocyanate to 150g of poly-1,4-butylene adipate diol (Mn=2000) and react at 80°C for 120 minutes;
[0117] (2) Add 45g of acetone, control the temperature of the reaction system at 50°C, add 11.25g of dimethylol propionic acid and 12.96g of N,N-di(2-hydroxyethyl)aminomethylphosphonic acid dimethyl, React at 75°C for 180 minutes until the NCO value drops to 1.5% by weight;
[0118] (3) Control the temperature of the reaction system at 40° C., add 8.45 g of triethylamine for neutralization reaction for 30 minutes;
[0119] (4) adding the neutralized and hydrophilic prepolymer into 350g deionized water for high-speed emulsification and dispersion to obtain a water-based polyurethane dispersion with a solid content of 40%;
[0120] (5) Add 4...
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