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Metal-base film thermocouple and preparation method thereof

A production method and technology of thermocouples, applied in thermoelectric device components, manufacturing/processing of thermoelectric devices, thermometers using electric/magnetic elements directly sensitive to heat, etc., can solve the problem of affecting measurement accuracy, consistency and reliability Poor performance, large insulation layer thickness and other problems, to achieve the effect of improving consistency and reliability, reliable design basis, and improving insulation performance

Inactive Publication Date: 2010-11-24
UNIV OF ELECTRONIC SCI & TECH OF CHINA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

This kind of thin-film thermocouple uses alumina ceramics as the insulating layer, which has the following problems: the insulating performance of the alumina ceramic layer is relatively poor, and the texture is loose. In order to ensure sufficient insulation, it is usually necessary to use thicker (about 20 μm) alumina. Ceramics are used as an insulating layer; what is more unfavorable is the thermal conductivity of alumina ceramic materials {The thermal conductivity refers to the temperature difference between the two sides of a 1m thick material is 1 degree (K, ℃) under stable heat transfer conditions, in 1 second The heat transferred through an area of ​​1 square meter within the bell, the unit is w (watt) / m K or ℃ (meter degree)} is low, only about 10W / m K, resulting in a gap between the surface temperature of the heat insulating layer and the substrate There is a large difference in the actual temperature, resulting in a large measurement error, which affects the accuracy of the measurement and the parameters provided as the basis for the design; Affect measurement accuracy
Therefore, due to the poor thermal conductivity and insulation of alumina ceramics and the large thickness of the required insulating layer in the above-mentioned background technology, there is a large difference between the actual temperature of the metal substrate and the surface temperature of the insulating layer and poor measurement accuracy in actual measurement, resulting in The consistency and reliability of the temperature measured by the thermocouple and the actual temperature of the metal substrate to be tested are poor, and the accuracy of using it as a design parameter is poor and other defects

Method used

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Embodiment Construction

[0020] Take the K-type NiCr-NiSi thermocouple film sensor prepared on a nickel (Ni)-based alloy substrate as an example:

[0021] 1) A nickel (Ni)-based alloy of (length×width×thickness) 30×95×5 mm was used as the substrate 1 to be tested, and after being ultrasonically cleaned with acetone and ethanol in sequence, it was dried under a nitrogen atmosphere;

[0022] 2) Put the cleaned Ni-based alloy substrate 1 in a vacuum of 6.0×10-4 In Pa vacuum (i.e. background vacuum) environment, NiCrAlY alloy is used as the target material, and argon gas with a purity of 99.999% is input as the sputtering medium at a temperature of 600°C, a power of 200W, and a sputtering pressure (working pressure) of 0.5Pa Under the condition of , the NiCrAlY alloy is deposited on the Ni-based alloy substrate by the DC magnetron sputtering method, and the deposition thickness is 10 μm, so as to obtain a composite substrate covering the NiCrAlY alloy transition layer 2;

[0023] 3) Put the composite subs...

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Abstract

The invention belongs to a metal-base film thermocouple and a preparation method thereof. The thermocouple comprises a metal substrate to be tested and a NiCrAlY alloy transitional layer arranged on the top face of the metal substrate, wherein a metal aluminum layer, an AlN layer, an AlN ceramic insulation layer, a thermocouple film electrode assembly and an aluminum oxide protective layer are formed on the transitional layer in turn. The production method comprises: processing the metal substrate to be tested; preparing a composite substrate with the NiCrAlY alloy transitional layer; precipitating metal aluminum; nitriding the aluminum; sputtering and depositing the AlN insulation layer; and setting the film thermocouple group and covering the aluminum oxide protective layer. In the invention, the AlN ceramic material with high coefficient of heat conductivity and high insulating performance is used as the insulation layer, so the temperature difference between the metal substrate and the surface of the insulation layer and the thickness of the insulation layer are reduced considerably; and thus, the metal-base film thermocouple has the characteristics of effectively reducing measurement error, improving the consistency between the temperature measured by the thermocouple and the actual temperature of the metal substrate to be tested, improving reliability, providing accurate and reliable basis for the design of turbine engines, and the like.

Description

technical field [0001] The invention belongs to the field of sensor production technology and measurement technology for turbine blades, in particular to a thin-film thermocouple made of turbine engine blades to be measured as a substrate (material) and a production method thereof. This type of thermocouple can be widely used in Measure the surface temperature distribution of turbine engine blades, combustion chambers, etc., and provide corresponding basic data basis for the design of turbine engines. Background technique [0002] In modern aero-engine technology, the harsh gas environment such as high temperature and high pressure generated by gas combustion will cause the surface temperature of the turbine blade and the combustion chamber to rise sharply, and at the same time generate a large thermal strain, while the temperature of the turbine blade and the surface of the combustion chamber The distribution and thermal strain have a great influence on the performance and ...

Claims

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Application Information

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IPC IPC(8): H01L35/28H01L35/02H01L35/34G01K7/04
Inventor 蒋洪川张万里王从瑞陈寅之刘兴钊李言荣
Owner UNIV OF ELECTRONIC SCI & TECH OF CHINA
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