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High-strength viscose fiber and production method thereof

A viscose fiber, production method technology, applied in the direction of viscose-made rayon, cellulose/protein conjugated rayon, etc., can solve the problem of affecting the beauty of the fabric, the high shrinkage rate of the viscose fiber, and the inability to be strongly scrubbed. and other problems, to achieve the effects of excellent hygroscopicity and wearing comfort, controllable operation process, and simple and easy method.

Active Publication Date: 2012-01-18
QINGDAO TIANYI GROUP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Although viscose fiber has the above-mentioned series of advantages, its disadvantages are also obvious: the strength of viscose fiber is low, especially the wet strength is poor, only more than half of the dry strength, it cannot be scrubbed strongly when washing, and the service life is short The shrinkage rate of viscose fiber is high, and the appearance of the fabric after washing is not ideal; the elasticity of viscose fiber is poor, and it is easy to deform when worn, causing wrinkles, especially the elbow and knee parts of the clothes will have local arching, which will affect the appearance of the fabric

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • High-strength viscose fiber and production method thereof

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Embodiment 1

[0036] A kind of production method of high-strength viscose fiber, the bacterial cellulose of flake is placed in the vacuum oven of 100 ℃, bakes to constant weight; Then add the concentration and be 5% ethylenediamine solution After being mechanically stirred at room temperature for 2 hours, wash with distilled water first, then soak in ethanol for 3 times, each time for 30 minutes, and then bake in a vacuum oven at 100°C to constant weight; use the ball milling method to pulverize the above-mentioned sheet-shaped bacterial cellulose to obtain micro Nano-scale bacterial cellulose powder, under the action of ultrasonic waves, gradually add 2 grams of bacterial cellulose powder to 1000 grams of viscose spinning solution with a concentration of 10%, to obtain a mixed solution of the two, and then continue to Disperse for 50 minutes under the action of ultrasonic waves to obtain a uniformly dispersed mixed solution, vacuum defoam the mixed solution for 14 hours, and then use ordina...

Embodiment 2

[0038] A kind of production method of high-strength viscose fiber, place bacterial cellulose sheet in the vacuum oven of 80 ℃, dry to constant weight; Then add concentration and be in the ethylenediamine solution of 6%, the room temperature mechanical stirring process 1.5 After h, wash with distilled water first, then soak in ethanol for 3 times, each time for 30 minutes, filter and bake in a vacuum oven at 80°C to constant weight; use ball milling method to crush the above-mentioned flake bacterial cellulose to obtain micronano-scale bacterial fibers Plain powder, under the action of ultrasound, gradually add 4 grams of bacterial cellulose powder to 1000 grams of viscose solution with a concentration of 10%, to obtain a mixed solution of the two, and then continue to disperse for 60 minutes under the action of ultrasound to obtain Disperse the mixed solution evenly, vacuum defoam the mixed solution for 14 hours, and then adopt the production equipment and process of ordinary v...

Embodiment 3

[0040] A kind of production method of high-strength viscose fiber, place bacterial cellulose sheet in the vacuum oven of 90 ℃, dry to constant weight; Then add concentration and be 7% in the ethylenediamine solution, room temperature mechanical stirring process 1.2 After h, first wash with distilled water, then soak in ethanol for 3 times, each time for 30 minutes, filter and bake in a vacuum oven at 90°C to constant weight; use ball milling to pulverize the above-mentioned flake bacterial cellulose to obtain micronano-scale bacterial fibers Plain powder, under the action of ultrasound, gradually add 6 grams of bacterial cellulose powder to 1000 grams of viscose solution with a concentration of 10%, to obtain a mixed solution of the two, and then continue to disperse for 70 minutes under the action of ultrasound to obtain Disperse the mixed solution evenly, vacuum defoam the mixed solution for 14 hours, and then use ordinary viscose fiber production equipment and technology to ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention discloses a high-strength viscose fiber and a production method thereof, which are characterized in that the viscose fiber is formed by mixing bacterial cellulose and viscose spinning solution, wherein the content of the bacterial cellulose in the viscose fiber is 1 to 10 percent. The production method comprises the following steps: the flake bacterial cellulose is pre-processed, and then the flake bacterial cellulose after the preprocessing is smashed with a ball milling method to obtain a micro nano-grade bacterial cellulose powder; the bacterial cellulose powder is added intothe viscose spinning solution to be uniformly scattered and defoamed to obtain a spinning solution; and the spinning solution is made into a high-strength viscose fiber. The content of the bacterial cellulose in the viscose fiber is 1 to 10 percent. The viscose fiber which is prepared with the production method has high strength, small shrinkage and good elasticity, can be blended and interwoven with cotton, wool and other synthesized fibers to be used for the fields such as top-grade costume fabric and industrial textiles, and the like.

Description

technical field [0001] The invention relates to the technical field of viscose fiber production, in particular to a high-strength viscose fiber and a production method thereof. Background technique [0002] Viscose fiber is the earliest man-made fiber to achieve industrial production. As early as the end of the 19th century, three British scientists, Cross, Bevan and Beadle, invented the method for preparing cellulose xanthate and applied for a patent for the production process of viscose fiber. For more than 100 years, viscose fiber has been favored by consumers for a long time due to its comfortable wearing performance, and its output has always been the largest among cellulose fibers. Compared with synthetic fibers, the advantages of viscose fiber are mainly reflected in three aspects: Aspects: [0003] 1 Raw materials come from a wide range of sources and are renewable resources. Viscose fiber is a man-made fiber produced from natural cellulose as the main raw material...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F2/08D01F8/02
Inventor 张传杰朱平蔚鹏飞王柳
Owner QINGDAO TIANYI GROUP
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