Preparation of plant source glucosamine hydrochloride
A technology of glucosamine hydrochloride and plant source, which is applied in the preparation of amino sugars and sugar derivatives, chemical instruments and methods, etc., can solve the problems of mildew and corruption, water pollution, environmental pollution, etc., and achieves a simple and easy production process. Product quality is guaranteed and the effect of reducing production costs
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Embodiment 1
[0019] The preparation method of plant source glucosamine hydrochloride of the present invention adopts the following steps:
[0020] (1) Acid hydrolysis: In a closed acid-resistant container with a stirring device, first add 300 kg of mycelium produced in the process of producing citric acid by fermentation, then add 600 kg of hydrochloric acid with a mass concentration of 25%, and start stirring , the temperature rose to 65°C, and the reaction was held for 10 hours;
[0021] (2) Cooling and pressure filtration: cool the feed liquid after the above reaction to below 10°C, precipitate crystals from the feed liquid, filter to obtain a crude product, transfer it to another acid-resistant container, and add 1000 kg of Deionized water, heated under agitation to redissolve the crude product, and then press filter;
[0022] (3) Decolorization: transfer the filtrate after the above-mentioned pressure filtration into an acid-resistant container with stirring, add barium hydroxide acc...
Embodiment 2
[0027] The preparation method of plant source glucosamine hydrochloride of the present invention mainly adopts the following steps:
[0028] (1) Acid hydrolysis: In an airtight acid-resistant container with a stirring device, first add 600 kg of mycelia produced during the production of citric acid by fermentation, then add 800 kg of hydrochloric acid with a mass concentration of 20%, and start stirring , the temperature was raised to 50°C, and the reaction was kept for 15 hours;
[0029] (2) Cooling and pressure filtration: cool the feed liquid after the above reaction to below 10°C, precipitate crystals from the feed liquid, filter to obtain a crude product, transfer it to another acid-resistant container, and add 1200 kg of Deionized water, heated under agitation to redissolve the crude product, and then press filter;
[0030] (3) Decolorization: transfer the filtrate after the above-mentioned pressure filtration into an acid-resistant container with stirring, add barium c...
Embodiment 3
[0035] The preparation method of plant source glucosamine hydrochloride of the present invention mainly adopts the following steps:
[0036] (1) Acid hydrolysis: In a closed acid-resistant container with a stirring device, first add 800 kg of mycelium produced in the process of producing citric acid by fermentation, then add 1200 kg of hydrochloric acid with a mass concentration of 30%, and start stirring , the temperature rose to 80°C, and the reaction was held for 9 hours;
[0037] (2) Cooling and pressure filtration: cool the feed liquid after the above reaction to below 10°C, precipitate crystals from the feed liquid, filter to obtain a crude product, transfer it to another acid-resistant container, and add 1500 kg of Deionized water, heated under agitation to redissolve the crude product, and then press filter;
[0038] (3) Decolorization: transfer the filtrate after the above-mentioned pressure filtration into an acid-resistant container with stirring, add barium chlori...
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