Concrete surface protecting material and method of manufacturing the same
A technology for concrete surface and protective materials, applied in the field of concrete surface protective materials, can solve problems such as examples and research of anhydrous concrete projects, affecting the functions of water conservancy and hydropower projects, and national economic losses, achieving excellent mechanical properties and facilitating secondary repairs , the effect of increasing the solid content
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[0034]The concrete surface protection material of the present invention, it is made up of A component and B component, it is characterized in that described A component comprises polyaspartic acid ester, inorganic nanometer material, silane coupling agent, reactive diluent, described B The component is a curing agent, and the mass content of the raw material components is: 60-120 parts of polyaspartic acid ester, 1-50 parts of inorganic nanomaterials, 0.001-10 parts of silane coupling agent, 5-100 parts of reactive diluent parts, curing agent 30 to 250 parts. The preparation method of the polyaspartic acid ester comprises the following steps: ① adding 40-100 parts of difunctional primary amine into the reaction kettle; ② slowly adding 40-100 parts of maleic acid ester or fumaric acid while stirring Ester, and keep the temperature at about 30-40°C; ③ Vacuumize the reactor so that the pressure inside the reactor is -0.1MPa, and then fill the reactor with nitrogen to make the pre...
Embodiment 1
[0066] Preparation of concrete surface protection material CKT-A.
[0067] Add 40 parts of 3,3'-dimethyl 4,4'-dicyclohexylmethanediamine into the reaction kettle, slowly add 57.8 parts of diethyl maleate while stirring, and keep the temperature at about 30°C . Vacuumize the reactor so that the pressure inside the reactor is -0.1MPa, then fill the reactor with nitrogen to make the pressure inside the reactor zero, and do this 2 to 3 times. Continue to stir, raise the temperature to 90°C, and react for about 12 hours to obtain polyaspartic acid ester.
[0068] Select the curing agent 2,4-, 2,6-toluene diisocyanate mixture (TDI) and diphenylmethane diisocyanate (MDI) in a ratio of 1:10 at room temperature and mix well with a mixer.
[0069] Select reactive diluents ethylene glycol and propylene glycol at a ratio of 1:10 and mix thoroughly with a mixer at room temperature.
[0070] Add 15 parts of nano-SiO to 60 parts of polyaspartate 2 , 2 parts of silane coupling agent KH550...
Embodiment 2
[0074] Preparation of concrete surface protection material CKT-B.
[0075] Add 58.4 parts of dicyclohexylmethanediamine into the reaction kettle, slowly add 80 parts of dimethyl maleate while stirring, and keep the temperature at about 40°C. Vacuumize the reactor so that the pressure inside the reactor is -0.1MPa, then fill the reactor with nitrogen to make the pressure inside the reactor zero, and do this 2 to 3 times. Continue to stir, raise the temperature to 100°C, and react for about 10 hours to obtain polyaspartic acid ester.
[0076] Select the curing agent isophorone-diisocyanate (IPDI) and 1,6-hexamethylene diisocyanate (HDI) in a ratio of 10:1 and mix thoroughly with a mixer at room temperature.
[0077] The active diluent ethylene glycol and polyethylene glycol are selected to be fully mixed with a mixer at room temperature at a ratio of 10:1.
[0078] Add 20 parts of nano-CaCO to 80 parts of polyaspartate 3 , 2 parts of silane coupling agent KH151 and 50 parts of ...
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