MgO-SiC-C material synthesized by forsterite-C and method for preparing same
A technology of forsterite and olivine mineral powder, which is applied in the field of MgO-SiC-C material and its preparation, can solve the problems affecting the high-temperature strength and erosion resistance of materials, the shortage of magnesia resources, and the increase of production cost, and achieve Excellent anti-slag performance, solve the shortage of resources, and prolong the service life
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Embodiment 1
[0014] A method for preparing a forsterite-C synthesized MgO-SiC-C material. First mix 1-1.3mol of forsterite ore powder and 3-3.5mol of C powder according to the molar ratio, add 7-8wt% sodium lignosulfonate and calcium sulfonate of the above-mentioned mixture and prepare an aqueous solution, stir for 10 ~30 minutes, and then dried at 60~90°C for 18~24 hours after compression molding. Then sinter in reducing atmosphere, the sintering temperature is 1680-1700°C, and the holding time is 3-4 hours to obtain MgO-SiC-C composite material.
[0015] Among them: the MgO content of the forsterite mineral powder is ≥38%, and the particle size is 0.2-0mm; the C content of the industrial carbon powder is ≥80%, and the particle size is 0.1-0mm.
Embodiment 2
[0017] A method for preparing a forsterite-C synthesized MgO-SiC-C material. Mix 1-1.5mol of forsterite ore powder and 3.5-4mol of C powder according to the molar ratio, add 7-7.8wt% sodium lignin sulfonate and calcium sulfonate of the above mixture and make it into an aqueous solution, mix and grind 10 to 30 minutes, and then dried at 60 to 90°C for 18 to 24 hours after compression molding. Then sinter in reducing atmosphere, the sintering temperature is 1650-1700°C, and the holding time is 2-3 hours, to obtain MgO-SiC-C composite material. All the other are with embodiment 1.
Embodiment 3
[0019] A method for preparing a forsterite-C synthesized MgO-SiC-C material. First mix 1-1.5mol of forsterite ore powder and 4-4.5mol of C powder according to the molar ratio, add 8-9wt% sulfurous acid pulp waste liquid of the above-mentioned mixture and make it into an aqueous solution, and mix and grind for 10-30 minutes , After being pressed and formed, it is naturally dried indoors for 24 to 36 hours. Then sintering in a reducing atmosphere, the sintering temperature is 1500-1550°C, and the holding time is 6-7 hours to obtain a MgO-SiC-C composite material. All the other are with embodiment 1.
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