Soldering paste and its preparation method
A solder paste and solder powder technology, applied in welding equipment, welding media, manufacturing tools, etc., can solve the problems of incomplete and bright solder joints, poor adaptability of lead-free solder paste, and color and luster of residue residues, and achieve full solder joints. Bright, adaptable, no-clean effect
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Embodiment 1
[0023] Taking the preparation of 1000 grams of solder paste as an example, this preparation method includes the following steps in sequence:
[0024] (1) Weigh alloy solder powder Sn 96.5 Ag 3.0 Cu 0.5 827.5 grams, 60 grams of organic solvents (of which 50 grams of nitromethane, 5 grams of ethanol, and 5 grams of methanol), 68 grams of organic acids (of which 8 grams of oxalic acid, 7 grams of glutaric acid, 21 grams of malonic acid, dodeca 32 grams of diacid), 30 grams of resin (wherein 20 grams of water-white hydrogenated rosin, 10 grams of turpentine) and 14.5 grams of surfactants (wherein 13 grams of TX-10 phosphate, 1.5 grams of fully hydrogenated castor oil); and prepare a dry , clean reaction vessel;
[0025] (2) Add the above-mentioned organic solvent into the reaction vessel, heat and stir at the same time, so that the material inside the reaction vessel is evenly heated to 130°C to 132°C;
[0026] (3) Keep the temperature of the reaction vessel at 130°C to 132°C...
Embodiment 2
[0031] Taking the preparation of 1000 grams of solder paste as an example, this preparation method includes the following steps in sequence:
[0032] (1) Weigh alloy solder powder Sn 99 Ag 0.3 Cu 0.7 850 grams, 80 grams of organic solvents (including 30 grams of dipropylene glycol methyl ether, 30 grams of ethylene glycol, and 20 grams of butyl acetate), 15 grams of organic acids (including 5 grams of methylene succinic acid, p-tert-butyl benzoic acid 10 grams), resin 50 grams (wherein 40 grams of perhydrogenated rosin, polymerized rosin 5 grams, hydrogenated rosin methyl ester 5 grams) and surfactant 5 grams (wherein polyethylene glycol 2 grams, nonylphenol polyoxyethylene ether 2 grams, 1 gram of alkylphenol polyoxyethylene ether); and prepare a dry, clean reaction vessel;
[0033] (2) Add the above-mentioned organic solvent into the reaction vessel, heat and stir at the same time, so that the material inside the reaction vessel is evenly heated to 135°C to 137°C;
[00...
Embodiment 3
[0039] Taking the preparation of 1000 grams of solder paste as an example, this preparation method includes the following steps in sequence:
[0040] (1) Weigh alloy solder powder Sn 95.5 Ag 4.0 Cu 0.5885 grams, 65 grams of organic solvent (of which 65 grams of tetrahydrofurfuryl alcohol), 27 grams of organic acid (of which 4 grams of succinic anhydride, 5 grams of dodecanoic acid, 13 grams of hexadecanoic acid, 5 grams of benzoic acid), 20 grams of resin (wherein 20 grams of hydrogenated rosin) and 3 grams of surfactants (wherein 1 gram of butylene glycol, 1 gram of polyethylene glycol, and 1 gram of castor oil polyoxyethylene ether); and prepare a dry, clean reaction vessel;
[0041] (2) Add the above-mentioned organic solvent into the reaction vessel, heat and stir at the same time, so that the material inside the reaction vessel is evenly heated to 137°C to 139°C;
[0042] (3) Keep the temperature of the reaction vessel at 137°C to 139°C, while stirring, add the above-m...
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