Super high flowing, white, fire retardant PBT with no halogen, in high thermal stability, and preparation method
A high thermal stability, white technology, applied in ultra-high flow, high thermal stability white halogen-free flame retardant PBT and production field, can solve phosphorus instability, extrusion production is easy to foam, PBT long-term effect can not meet the use requirements etc. to achieve good mechanical properties and high thermal stability
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Embodiment 1
[0035] First bake the polybutylene terephthalate (PBT) of 73.6% by weight at 120-150°C (example 120°C, 135°C, 150°C) for 2-5 hours (example 2, 4, 5 hours), Control the water content below 0.05%; then mix it with 20% by weight of the composite flame retardant through a mixer or separately enter the twin-screw extruder from the metering feeder to plasticize and melt, and add it to the twin-screw extruder at the same time 6% by weight of toughener methacrylate butadiene styrene terpolymer and 0.2% by weight of primary antioxidant (1010) pentaerythritol tetra-3-(3,5-di-tert-butyl-4 hydroxybenzyl ) propionate, 0.2% by weight of auxiliary antioxidant (168) tris ((2,4-di-tert-butylphenyl) phosphite, and then through conventional extrusion, drawing, cooling, pelletizing, homogenizing , Packaging products.
[0036] The preparation method of the composite flame retardant is as follows: first add nano-kaolin to the high mixer and mix, and simultaneously heat up to 70-150°C (example 70°C...
Embodiment 2
[0038]First bake 49.6% by weight of polybutylene terephthalate (PBT) at 120-150°C (example 120°C, 135°C, 150°C) for 2-5 hours (example 2, 4, 5 hours), Control the water content below 0.05%; then mix with 16% by weight of composite flame retardant through a mixer or separately enter the twin-screw extruder from the metering feeder to plasticize and melt, and add it to the twin-screw extruder at the same time The toughener methacrylate butadiene styrene terpolymer of 4% by weight, the alkali-free glass fiber of 30% by weight and the primary antioxidant (1010) pentaerythritol four 3-(3,5- Di-tert-butyl-4-hydroxybenzyl) propionate, 0.2% by weight of auxiliary antioxidant (168) tris ((2,4-di-tert-butylphenyl) phosphite, and then through conventional extrusion, drawing strips, cooled, diced, homogenized, and packaged to obtain products.
[0039] The preparation method of the composite flame retardant is as follows: first add nano-kaolin to the high mixer and mix, and simultaneously...
Embodiment 3
[0044] First bake 85% by weight of polybutylene terephthalate (PBT) at 120-150°C (example 120°C, 135°C, 150°C) for 2-5 hours (example 2, 4, 5 hours), Control the moisture below <0.05%; then mix with 8% by weight of composite flame retardant (3% by weight of organic phosphonate, 2% by weight of nano-kaolin, 3% by weight of silicone) through a mixer or separately Enter the twin-screw extruder from the metering feeder for plasticization and melting, and at the same time add 7% by weight of toughening agent methacrylate butadiene styrene terpolymer to the twin-screw extruder, and then extrude through conventional , stranding, cooling, dicing, mixing, and packaging. All the other are with embodiment 1.
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