Multiple-phase ceramic material and method for manufacturing same
A technology of composite phase ceramics and manufacturing methods, which is applied in the field of ceramic materials, can solve the problems of high speed-up smoke, slow car speed-up, blade fracture and failure, etc., and achieve the goal of increasing compression ratio, reducing loose packing ratio, and improving consistency Effect
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Embodiment 1
[0030] 1) Ingredients
[0031] Weigh 50 parts of ZrO by weight 2 powder, 20 parts of TiAl powder, 20 parts of Al 2 o 3 Powder, 5 parts of Ti powder and 5 parts of Al powder constitute raw materials;
[0032] 2) Mixing and grinding
[0033] The raw materials are mixed and ground to obtain a mixed powder. Said mixing and grinding steps are carried out in a planetary mill.
[0034] Ball milling is the basic method used in mineral processing ceramics, and its main functions are particle size reduction, solid state alloying, mixing or fusion and changing the shape of ions. The planetary grinding machine is composed of a ball mill tank, a tank seat, a turntable, a fixed pulley and an electric motor. The working principle is: the planetary grinder is equipped with 4 ball milling pots on the turntable. When the turntable rotates, the ball milling pots make planetary motion around the same axis with the turntable, and the abrasives in the pots are ground and mixed in high-speed m...
Embodiment 2
[0053] It is basically the same as Example 1, the difference is:
[0054] When batching, the ratio of each component that constitutes the raw material is different, see Table 1;
[0055] When granulating, add a polyvinyl alcohol aqueous solution with a concentration of 20% as a plasticizer in a weight ratio equivalent to 5% of the mixed powder;
[0056] When stewing the material, the pellets were aged for 22 hours;
[0057] When molding, the molding pressure is 170MPa, and the holding time is 5 minutes;
[0058] During sintering, the sintering route is: 550°C → 1650°C → 1650°C, the heating rate is 160°C / hour, the heat preservation is 2h; the nitrogen atmosphere is 2MPa.
[0059] The performance parameters of the composite ceramic materials after sintering are shown in Table 2 and Table 3.
Embodiment 3
[0061] Basically the same as Example 1, the difference is that,
[0062] When batching, the ratio of each component that constitutes the raw material is different, see Table 1;
[0063] When granulating, add a polyvinyl alcohol aqueous solution with a concentration of 20% as a plasticizer in a weight ratio equivalent to 10% of the mixed powder;
[0064] When stewing the material, the pellets were aged for 16 hours;
[0065] When molding, the molding pressure is 190MPa, and the holding time is 6 minutes;
[0066] During sintering, the sintering route is: 550°C → 1700°C → 1700°C, the heating rate is 170°C / hour, the heat preservation is 2h; the nitrogen atmosphere is 2MPa.
[0067] The performance parameters of the composite ceramic materials after sintering are shown in Table 2 and Table 3.
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