Method for producing benzene aromatic hydrocarbon from crude benzole
A technology for benzene series aromatic hydrocarbons and crude benzene, which is applied in chemical instruments and methods, purification/separation of hydrocarbons, hydrocarbons, etc., can solve the problems of difficult long-term operation, unstable crude benzene, easy polymerization, etc., and achieves adaptability Strong, extended operation cycle, high purity effect
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Embodiment 1
[0025] Crude benzene raw material 1, whose properties are shown in Table 1, enters the hydrogenation reactor 1 after being mixed with hydrogen, and the reaction conditions are shown in Table 2. The catalyst is a molybdenum-nickel hydrogenation catalyst, and the gas-liquid mixture discharged from the hydrogenation reactor enters the gas-liquid separation Device 2. The liquid phase is sent to the stripper 3, and the liquid product is collected after stripping, which is called hydrogenated oil. The properties and group composition of the hydrogenated oil are shown in Table 2. Hydrogenated oil is pre-distilled to separate heavy components containing xylene and light components containing benzene, toluene and non-aromatics. The former is sent to rectification to obtain petroleum grade mixed xylene, and the latter is extracted with N-formylmorpholine Distillation to separate non-aromatic hydrocarbons and rich solvents containing benzene and toluene. The rich solvents are then rectif...
Embodiment 2
[0027] Crude benzene raw material 2, its properties are shown in Table 1. See Table 2 for hydrogenation reaction conditions, properties and family composition of hydrogenated oil. Other reaction conditions, reaction steps are with embodiment 1. The product properties are shown in Table 3.
Embodiment 3
[0029] Crude benzene raw material 3, its properties are shown in Table 1. See Table 2 for hydrogenation reaction conditions, properties and family composition of hydrogenated oil. Other reaction conditions, reaction steps are with embodiment 1. The product properties are shown in Table 3.
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