Antibacterial and health-caring feedstuff addictive and preparation method thereof
The technology of feed additive and montmorillonite is applied in the field of health care feed additive and its preparation and antibacterial, which can solve the problems of loss of antibacterial activity and high product cost, and achieve the effects of inhibiting proliferation, improving production performance and reducing animal diarrhea rate.
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Embodiment 1
[0018] 1) Add montmorillonite minerals, together with sodium chloride equivalent to 5% of the mineral weight, add water and stir evenly to make a suspension slurry with a concentration of 20%, sodiumize at room temperature for 10 hours, wash with water 5 times, and remake the concentration with water 20% pulp;
[0019] 2) Copper chloride with a copper content of 0.5% of the weight of the montmorillonite mineral and zinc chloride with a zinc content of 1% of the weight of the montmorillonite mineral are slowly added to the slurry of step 1) under stirring, and are detected and adjusted The pH value of the pulp is 3.5, and it is reacted at room temperature for 5 hours;
[0020] 3) In the detection step 2) the pH value of the pulp is adjusted with 10moL / L sodium hydroxide aqueous solution, so that the pH value of the slurry is 7.0; washed 3 times with water, filtered and dehydrated;
[0021] 4) drying and pulverizing the filter cake obtained in step 3) to 300 mesh to obtain an a...
Embodiment 2
[0023] 1) Add montmorillonite mineral, together with sodium chloride equivalent to 15% of the mineral weight, add water and stir evenly to make a suspension slurry with a concentration of 10%, sodiumize at room temperature for 15 hours, wash with water 7 times, and remake the concentration with water 10% pulp;
[0024] 2) Copper sulfate pentahydrate (CuSO 4 ·5H 2 (2) and zinc nitrate with a zinc content of 10% by weight of montmorillonite minerals are slowly added to the slurry of step 1) under stirring, and the pH value of the slurry is detected and adjusted to be 6.5, and reacted at room temperature for 10 hours;
[0025] 3) In the detection step 2) the pH value of the pulp is adjusted with 0.5moL / L potassium hydroxide aqueous solution, so that the pH value of the slurry is 8.5; washed 7 times with water, and centrifuged for dehydration;
[0026] 4) drying and pulverizing the filter cake obtained in step 3) to 400 mesh to obtain an antibacterial and health-care feed additi...
Embodiment 3
[0028] 1) Add montmorillonite minerals, together with sodium chloride equivalent to 10% of the mineral weight, add water and stir evenly to make a suspension slurry with a concentration of 15%, sodiumize at room temperature for 12 hours, wash with water 6 times, and remake the concentration with water 15% pulp;
[0029] 2) Copper sulfate with a copper content of 2.5% by weight of montmorillonite minerals and zinc sulfate heptahydrate (ZnSO4) with a zinc content of 4% by weight of montmorillonite minerals 4 ·7H 2 (0), slowly add in the pulp of step 1) under stirring, detect and adjust the pH value of the pulp to be 5.0, and react at room temperature for 8 hours;
[0030] 3) In the detection step 2) the pH value of the pulp is adjusted with 5moL / L sodium carbonate aqueous solution to make the pH value of the slurry 8.5; washed 6 times with water, filtered or centrifugally dehydrated;
[0031] 4) drying and pulverizing the filter cake obtained in step 3) to 500 mesh to obtain a...
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