Manganese supplementing feed additive having controlled slow-release type manganese, its preparation and use method
A feed additive, slow-release manganese technology, applied in animal feed, animal feed, application and other directions, can solve problems such as hindering the absorption and utilization of manganese, and achieve the effects of improving egg quality, preventing bone tissue damage, and improving feed returns.
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Embodiment 1
[0035] 1) Grinding a commercially available ZSM-5 zeolite molecular sieve to 300 mesh, adding water and stirring evenly to make a suspension slurry with a concentration of 5%;
[0036] 2) Slowly add manganese chloride with a manganese content of 5% by weight of zeolite into the suspension slurry in step 1) under stirring, detect and adjust the pH value of the slurry to 4.5, and react at room temperature for 6 hours;
[0037] 3) The pH value of the detection step 2) is adjusted with a 10moL / L aqueous sodium hydroxide solution to make the pH value of the slurry 7.5; washed with water for 3 times, filtered and dehydrated;
[0038] 4) The filter cake obtained in step 3) is dried and crushed to 300 meshes to obtain a controlled and slow-release manganese supplement, and the content of manganese in the zeolite is 5% by weight percentage.
[0039] Study on the bioavailability of different forms of manganese sources to broiler chickens:
[0040]A 3×4 two-factor completely randomized ...
Embodiment 2
[0047] 1) Grinding the clinoptilolite produced in Jinyun, Zhejiang to 500 mesh, adding water and stirring evenly to make a suspension slurry with a concentration of 10%;
[0048] 2) Slowly add manganese acetate containing 2% by weight of zeolite into the suspension slurry in step 1) under stirring, detect and adjust the pH value of the slurry to 3.0, and react at room temperature for 4 hours;
[0049] 3) The pH value of the detection step 2) is adjusted with 0.5moL / L sodium carbonate aqueous solution, so that the pH value of the slurry is 7.0; washed 4 times, filtered and dehydrated;
[0050] 4) The filter cake obtained in step 3) is dried and crushed to 600 meshes to obtain a controlled and slow-release manganese supplement, and the content of manganese in the zeolite is 2% by weight percentage.
[0051] Effects of manganese sources and levels on growth performance and tissue manganese content of Penaeus vannamei:
[0052] 1. Experimental design
[0053] The experiment adop...
Embodiment 3
[0063] Preparation: Mesoporous molecular sieve MCM-41 was prepared according to the method of "Modification and Characterization of Mesoporous Molecular Sieve MCM-41 under Mild Conditions" (Zheng Shan, Gao Lian, Guo Jingkun. Journal of Inorganic Materials, 2000, 15(5): 844-848). 41.
[0064] 1) Grind the mesoporous molecular sieve MCM-41 obtained in the preparatory step to 300 mesh, add water and stir evenly, and make a suspension slurry with a concentration of 1%;
[0065] 2) Slowly add manganese nitrate with a manganese content of 10% by weight of MCM-41 into the suspension slurry in step 1) under stirring, detect and adjust the pH value of the slurry to 6.5, and react at room temperature for 10 hours;
[0066] 3) The pH value of the detection step 2) is adjusted with 5moL / L potassium hydroxide aqueous solution, so that the pH value of the slurry is 8.5; washed 5 times with water, and centrifuged for dehydration;
[0067] 4) The filter cake obtained in step 3) was dried and...
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