Process for preparing permanent magnet iron oxygen body polymer composite magnet
A technology of permanent magnet ferrite and composite magnet, applied in the direction of magnetism of organic materials/organic magnetic materials, etc., can solve the problems of complex process, low mixing efficiency, and high mixing equipment and process requirements, to simplify the preparation process, overcome the mixed Equipment and process demanding effects
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Embodiment 1
[0023] In terms of parts by mass, 3 parts of KH550 and 100 parts of strontium ferrite magnetic powder are mixed evenly and then fully dried, and the surface of the magnetic powder is coated. Subsequently, in parts by mass, 6 parts of dibenzoyl peroxide were added to 100 parts of methyl methacrylate monomer to make methyl methacrylate monomer solution; 10 parts of monomer solution was mixed with the above Mix 90 parts of strontium ferrite magnetic powder after one-step treatment to prepare a suspension system, then heat the suspension system to 90°C in nitrogen and keep it warm for 8 hours to make the methyl methacrylate monomer undergo in-situ polymerization on the surface of the magnetic powder Polymethyl methacrylate is produced. Finally, using a twin-screw extruder at 190°C, the magnetic powder coated with polymethyl methacrylate is directly extruded under the action of a 1000kA / m orientation magnetic field to prepare the strontium ferrite powder-polymethyl methacrylate Es...
Embodiment 2
[0025] In terms of parts by mass, 6 parts of KH550 and 100 parts of strontium ferrite magnetic powder were mixed evenly and then fully dried, and the surface of the magnetic powder was coated; Add 7 parts of azobisisobutyronitrile in the glyceride monomer to make methyl methacrylate glycidyl ester monomer melt; and 10 parts of monomer solution with 90 parts of strontium iron Oxygen and magnetic powder are mixed to prepare a suspension system; the suspension system is heated to 70°C in nitrogen and kept for 7 hours, so that methyl methacrylate glycidyl ester monomer undergoes in-situ polymerization reaction on the surface of the magnetic powder to form polymethyl methacrylate Ester glycidyl ester. Finally, using a single-screw extruder at 130°C, the magnetic powder coated with polymethyl methacrylate glycidyl ester was directly extruded under the action of a 1000kA / m orientation magnetic field to prepare the strontium ferrite powder-polymethacrylate Glycidyl methyl acrylate co...
Embodiment 3
[0027] In terms of parts by mass, 5 parts of KH550 and 100 parts of strontium ferrite magnetic powder are mixed uniformly, then fully dried, and the surface of the magnetic powder is coated. Subsequently, in terms of parts by mass, 6 parts of azobisisobutyronitrile were added to 100 parts of butyl acrylate to make a butyl acrylate melt; Parts of strontium ferrite magnetic powder were mixed to prepare a suspension system; the suspension system was heated to 65°C in nitrogen, and kept for 5 hours, so that the butyl acrylate monomer was in-situ polymerized on the surface of the magnetic powder to form polybutyl acrylate. Finally, using a twin-screw extruder at 120 ° C, the polybutyl acrylate-coated magnetic powder formed by polymerization is directly extruded under the action of an orientation magnetic field of 1000 kA / m to prepare the strontium ferrite powder-polybutyl acrylate Ester composite magnets. After testing, the maximum magnetic energy product of the prepared composite...
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