Method for making PH value-sensitive polyvinylidene fluoride hollow fibre intelligent film and products thereby
A polyvinylidene fluoride and smart membrane technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation, etc., to achieve the effects of improving hydrophilicity, easy industrial implementation, and easy cleaning
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Embodiment 1
[0028] (1) Pure water soaking membrane: Soak the dry polyvinylidene fluoride hollow fiber membrane in pure water for 24 hours, so that the surface of the membrane pores is completely infiltrated by water;
[0029] (2) Alkali-treated membrane: 500 ml of KOH solution with a concentration of 70 g was prepared, and 1.7 g of tetrabutylammonium bromide was added to the solution. Put the PVDF membrane into the prepared alkali solution, heat it in a water bath, the reaction temperature is 50°C, and the reaction time is 20 minutes. After alkali treatment, wash the KOH on the surface of PVDF with pure water for use;
[0030] (3) Manufacture composite membrane: prepare 200ml of acrylic acid solution with a concentration of 1mol / L, add 10ml of dimethylformamide solution and mix evenly; put the PVDF hollow fiber membrane treated with alkali into the mixed solution, soak at room temperature for 15 minutes;
[0031] Preparation contains cross-linking agent N, N-methylenebisacrylamide (MBAA)...
Embodiment 2
[0033] (1) with embodiment 1;
[0034] (2) Alkali-treated membrane: 500 ml of KOH solution with a concentration of 60 g was prepared, and 2 g of tetrabutylammonium bromide was added to the solution. Put the PVDF hollow fiber membrane into the prepared alkali solution, heat in a water bath, the reaction temperature is 80°C, and the reaction time is 1min. After alkali treatment, wash the KOH on the surface of PVDF with pure water for use.
[0035] (3) Manufacture of composite membrane: prepare 200 ml of acrylic acid solution with a concentration of 1.5 mol / L, add 10 ml of dimethylformamide solution and mix well. Put the alkali-treated PVDF hollow fiber membrane into the mixed solution and soak at room temperature for 10 minutes. Preparation contains cross-linking agent N, N-methylenebisacrylamide (MBAA) 0.1g and initiator potassium persulfate (K 2 S 2 o 8 ) 0.2g solution in 100ml. Put the acrylic acid-treated fiber membrane in the solution, filled with N 2 After sealing, ...
Embodiment 3
[0037] (1) with embodiment 1;
[0038] (2) Alkali-treated membrane: 500 ml of KOH solution with a concentration of 50 g was prepared, and 1.5 g of tetrabutylammonium bromide was added to the solution. Put the PVDF hollow fiber membrane into the prepared alkali solution, heat in a water bath, the reaction temperature is 70°C, and the reaction time is 10 minutes. After alkali treatment, wash the KOH on the surface of PVDF with pure water for use;
[0039] (3) Manufacture of composite membrane: Prepare 200 ml of acrylic acid solution with a concentration of 1.5 mol / L, add 8 ml of dimethylformamide solution and mix well. Put the alkali-treated PVDF hollow fiber membrane into the mixed solution and soak at room temperature for 10 minutes.
[0040] Preparation contains cross-linking agent N, N-methylenebisacrylamide (MBAA) 0.5g and initiator potassium persulfate (K 2 S 2 o 8 ) 0.2g solution in 100ml. Put the acrylic acid-treated fiber membrane in the solution, filled with N 2...
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