Pesticide water suspending nano capsule prepn and its preparing method
A technology for nanocapsules and pesticides, which is applied to the formulation of veterinary drugs and pesticides, can solve the problems of waste of resources, decomposition and waste, and low effective utilization rate, and achieve the effects of being beneficial to the ecological environment, improving stability, and improving utilization rate.
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Embodiment 1
[0056] 0.1g ammonium persulfate is dissolved in 20g water (divided into two parts by 4:1), stand-by; 0.5g pesticide active substance is dissolved in the mixed monomer of 7g styrene, 8g butyl acrylate, 0.2g acrylic acid; Dissolve 6g of OP-40 and 1g of sodium lauryl sulfate in 50g of 2% polyvinyl alcohol aqueous solution, put it into a stirring container, add the mixed monomers with pesticide active substances under stirring, and disperse into an emulsion , into the reaction vessel. Heat to keep the temperature at 70±2°C, add the first part of initiator, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1.5g of styrene, 1.5g of butyl acrylate, 2g of toluene diisocyanate mixed monomer and Add the second initiator dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, and discharge. The content of pesticide active substance in the product is 0.5%.
Embodiment 2
[0058]Dissolve 0.1g potassium persulfate in 10g water (divided into two parts according to 4:1), 1g acrylamide is dissolved in 10g water, stand-by; dissolve 1g pesticide active substance in 4g ethyl acrylate 7g butyl acrylate mixed monomer In; 5g OP-40, 4g sodium lauryl sulfate, 4g sodium polymethacrylate are dissolved in 60g water, put into a container with stirring, under stirring, add the mixed monomer that is dissolved in pesticide active matter, Disperse into an emulsion and put it into a reaction vessel. Heat and keep the temperature at 70±2°C, add the first initiator and acrylamide aqueous solution, react for 6 hours, keep warm for 1 hour, and prepare the seed emulsion; add 1g ethyl acrylate, 1g butyl acrylate, 2g 4,4' - diphenylmethane diisocyanate mixed monomer, dropwise for 1 hour, keep warm for 2 hours, cool down; add additives, discharge. The content of pesticide active substance in the product is 0.9%.
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