Method and apparatus for manufacturing a rare-earth metal doped optical fiber preform
A preform and equipment technology, applied in glass manufacturing equipment, light guides, manufacturing tools, etc., can solve problems such as difficult doping of rare earth dopants, achieve high pump power absorption, low core attenuation rate, numerical aperture small effect
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Embodiment 1
[0096] An optical fiber preform was prepared using the basic glass deposition components and parameters in Table 1.
[0097] cladding formation
(1450℃ hot zone, 3 passes)
(1450℃ hot zone, 4 passes)
components
flow
components
flow
SiCl 4
500cc / 20℃, 1.1g / min
SiCl 4
200cc / 22℃, 0.66g / min
GeCl 4
25cc / 20℃, 0.03g / min
POCl 3
687cc / 20℃, 0.16g / min
POCl 3
30cc / 20℃, 0.007g / min
SF 6
0.8cc / min
SF 6
0.25cc / min
O 2
1,000cc / min
O 2
1,000cc / min
he
1,000cc / min
he
1,000cc / min
[0098] * Sintered at 1960°C
[0099] More specifically, during the deposition process, a stream of glass-forming component vapor containing the above-mentioned components is introduced into the cavity of the quartz tube 5 through the outer delivery tube 240 of the multiple concentric delivery system 20 of FIG. 1, and reacts to form a powd...
Embodiment 1A-1C
[0103] Three kinds of optical fiber preforms (Examples 1A-1C) were prepared by the method of Example 1. However, the ytterbium chloride in Example 1A vaporizes at 930°C, in Example 1B at 950°C, and in Example 1C at 980°C. It is observed that the core depositions of Examples 1A-1C are the same, but the content of ytterbium oxide increases from 1A to 1C, that is, increases with the increase of gasification temperature. The concentration of ytterbium oxide in Example 1C exceeds 3 wt%. Example 1D
Embodiment 1D
[0104] An optical fiber preform was prepared by the method of Example 1. However, in this embodiment, the core layer is formed not by 4 passes but by 8 passes. The core composition of the obtained optical fiber preform is similar to that of the preform of Example 1, but the core diameter is larger, so it is more suitable for drawing multimode optical fiber. Example 1E
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