Cistanche pill production process, product and quality control method thereof

A quality control method, Cistanche pill technology, applied in the direction of pill delivery, medical preparations containing active ingredients, anti-inflammatory agents, etc., can solve the problem of inability to ensure the effect and quality, unable to fully and truly reflect the quality of Cistanche medicinal materials, and lack of simplicity It is easy to mass produce Cistanche medicinal materials, such as the method of quality standard control, to achieve the effect of avoiding water absorption and deterioration, and the production process is simple

Pending Publication Date: 2022-03-04
内蒙古祈蒙药业股份有限公司
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] However, when Cistanche deserticola is used as a unit medicinal material, there is a lack of a simple and easy production process that is conducive to mass production and a method for standardizing the quality of the medicinal material Cistanche deserticola. The existing production process and quality control methods cannot ensure the effect in the process and quality, so that it cannot fully and truly reflect the quality status of Cistanche medicinal materials

Method used

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  • Cistanche pill production process, product and quality control method thereof
  • Cistanche pill production process, product and quality control method thereof
  • Cistanche pill production process, product and quality control method thereof

Examples

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Effect test

preparation example Construction

[0050] Preparation of reference substance solution: take echinacoside and verbascoside to obtain a mixed reference substance, add methanol with a concentration of 50% to the mixed reference substance to form a mixed solution, and obtain a reference substance solution, wherein echinacoside and verbascoside The volume concentration of glycosides is 0.2mg / ml;

[0051] Preparation of the test solution: take 1g of Herba Cistanche, put it in a 100ml brown measuring bottle, add 50ml of methanol with a concentration of 50%, weigh it after shaking well, soak it for 30min, and ultrasonicate it under 250W power and 35kHz frequency After cooling for 40 minutes, weigh again, add methanol with a concentration of 50% to the brown measuring bottle to make up the weight lost by ultrasound, shake well, let it stand still, take the supernatant, filter, and take the subsequent filtrate to obtain the test product. product solution;

[0052] Determination of the content of echinacoside and verbasc...

Embodiment 1

[0061] A kind of production technology of cistanche pill, comprises the following steps:

[0062] Cistanche was washed and soaked in water under the following conditions: vacuum degree of 0.12MPa, temperature of 70°C, time of 40min, and then cut into 3mm slices to obtain Cistanche slices;

[0063] After pulverizing the cistanche tablets, pass through a 110-mesh sieve, and then mix for 60 minutes to obtain the medicinal powder;

[0064] After adding water to the above-mentioned medicinal powder, it is made into pellets;

[0065] The above-mentioned pellets are dried at 70° C. until the moisture content is 5%, and the finished Cistanche pills are obtained.

[0066] Carry out quality control to above-mentioned cistanche pill, comprise following detection item:

[0067] 1. Using echinacoside and verbascoside as index components, conduct a qualitative analysis of Cistanche pills by thin-layer chromatography. The specific steps are:

[0068] Take 1 g of Herba Cistanche pill, grin...

Embodiment 2

[0100] A kind of production technology of cistanche pill, comprises the following steps:

[0101] Cistanche was washed and soaked in water under the following conditions: a vacuum of 0.08 MPa, a temperature of 60°C, and a time of 30 minutes, and then cut into 3mm slices to obtain Cistanche slices;

[0102]After pulverizing the cistanche tablets, pass through a 100-mesh sieve, and then mix for 55 minutes to obtain the medicinal powder;

[0103] After adding water to the above-mentioned medicinal powder, it is made into pellets;

[0104] The above-mentioned pellets are dried at 60° C. until the moisture content is 7%, and the finished Cistanche pills are obtained.

[0105] Adopt the quality control method of embodiment 1 to detect the cistanche pill prepared in the present embodiment, and the detection result is a qualified product.

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Abstract

The invention provides a cistanche pill production process, a product and a quality control method thereof, and relates to the technical field of traditional Chinese medicine production quality detection. A production process of cistanche pills comprises the following steps: cleaning cistanche, soaking in water, and slicing to obtain cistanche slices; crushing the cistanche slices to obtain medicinal powder; adding water into the medicine powder, and preparing the medicine powder into pills; and drying the pills at 60-80 DEG C until the moisture content is less than or equal to 9% to obtain the finished product cistanche pills. The cistanche pills prepared by the production process disclosed by the invention are good in quality, the quality control method is good in specificity and good in reproducibility, and the inherent quality and the medication quality of the cistanche pills can be effectively evaluated and controlled.

Description

technical field [0001] The invention relates to the technical field of traditional Chinese medicine production quality detection, in particular to a production process, product and quality control method of Cistanche pills. Background technique [0002] Cistanche, the fleshy stem of Cistanche or Cistanche, Cistanche, etc., has a slight gas, sweet taste, and slightly bitter taste. It has the effects of nourishing the kidney, replenishing essence, moistening dryness and smoothing the intestines. It is mainly used to treat impotence in men and infertility in women. Leukorrhagia, blood metrorrhagia, cold pain in the waist and knees, blood dryness and constipation, etc. Cistanche can be used in combination with various medicinal materials, which can be used for the treatment of diseases, and can also be eaten as a health food. [0003] However, when Cistanche deserticola is used as a unit medicinal material, there is a lack of a simple and easy production process that is conduciv...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/64A61K9/20A61P15/10A61P15/08A61P15/00A61P7/04A61P29/00A61P1/10G01N30/90G01N30/02G01N30/36G01N33/15
CPCA61K36/64A61K9/20A61P15/10A61P15/08A61P15/00A61P7/04A61P29/00A61P1/10G01N30/90G01N30/02G01N30/36G01N33/15A61K2236/331A61K2236/15
Inventor 冯立宝徐佳枫员鹏飞
Owner 内蒙古祈蒙药业股份有限公司
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