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Sprayable hydrogel coating and preparation method of coating thereof

A technology of hydrogel and coating, applied in the direction of coating, etc., can solve the problem of high viscosity of hydrogel coating, achieve the effect of promoting hydrolysis, low equipment requirements, and low cost

Active Publication Date: 2021-08-13
HENAN UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This method obtains the hydrogel coating by directly coating the prepared gel coating on the solid surface, but because the viscosity of the hydrogel coating is too high, it is only suitable for preparing the hydrogel coating by brushing, dipping, etc. Floor
[0006] The above two methods are difficult to prepare uniform hydrogel coatings on solid surfaces with complex topography (such as hollows, gaps, etc.)

Method used

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  • Sprayable hydrogel coating and preparation method of coating thereof
  • Sprayable hydrogel coating and preparation method of coating thereof
  • Sprayable hydrogel coating and preparation method of coating thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0064] A kind of preparation method of sprayable hydrogel paint and coating thereof, is characterized in that, comprises the following steps:

[0065] S1. Synthesis of ultraviolet polymerization viscous solution:

[0066] Mix solvent, monomer, cross-linking agent and initiator in a reaction vessel to form a reaction solution, and carry out free radical polymerization reaction under ultraviolet light conditions to obtain a viscous solution for ultraviolet polymerization;

[0067] S2, solution dilution:

[0068] Dilute the ultraviolet polymerization viscous solution by adding ethanol to obtain a dilute solution that can be directly used for spraying;

[0069] S3, by adjusting the pH value of the dilute solution that can be directly used for spraying, adjust the curing time of the hydrogel coating:

[0070] Solution C is obtained by adding hydrochloric acid to adjust the pH value of the dilute solution which can be directly used for spraying;

[0071] S4, spraying and curing: ...

Embodiment 2

[0082] A kind of preparation method of sprayable hydrogel paint and coating thereof, is characterized in that, comprises the following steps:

[0083] S1. Synthesis of ultraviolet polymerization viscous solution:

[0084] Mix solvent, monomer, cross-linking agent and initiator in a reaction vessel to form a reaction solution, and carry out free radical polymerization reaction under ultraviolet light conditions to obtain a viscous solution for ultraviolet polymerization;

[0085] S2, solution dilution:

[0086] Dilute the ultraviolet polymerization viscous solution by adding ethanol to obtain a dilute solution that can be directly used for spraying;

[0087]S3, by adjusting the pH value of the dilute solution that can be directly used for spraying, adjust the curing time of the hydrogel coating:

[0088] Solution C is obtained by adding hydrochloric acid to adjust the pH value of the dilute solution which can be directly used for spraying;

[0089] S4, spraying and curing: ...

Embodiment 3

[0100] A kind of preparation method of sprayable hydrogel paint and coating thereof, is characterized in that, comprises the following steps:

[0101] S1. Synthesis of ultraviolet polymerization viscous solution:

[0102] Mix solvent, monomer, cross-linking agent and initiator in a reaction vessel to form a reaction solution, and carry out free radical polymerization reaction under ultraviolet light conditions to obtain a viscous solution for ultraviolet polymerization;

[0103] S2, solution dilution:

[0104] Dilute the ultraviolet polymerization viscous solution by adding ethanol to obtain a dilute solution that can be directly used for spraying;

[0105] S3, by adjusting the pH value of the dilute solution that can be directly used for spraying, adjust the curing time of the hydrogel coating:

[0106] Solution C is obtained by adding hydrochloric acid to adjust the pH value of the dilute solution which can be directly used for spraying;

[0107] S4, spraying and curing: ...

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Abstract

The invention discloses a sprayable hydrogel coating and a preparation method of the coating. The preparation method is characterized by comprising the following steps: S1, performing synthesis of an ultraviolet polymerization viscous solution: mixing a solvent, a monomer, a cross-linking agent and an initiator in a reaction container to form a mixed reaction solution, stirring and carrying out free radical polymerization reaction under the condition of ultraviolet illumination to obtain the ultraviolet polymerization viscous solution; s2, performing solution dilution: diluting the ultraviolet polymerization viscous solution by adding ethanol to obtain a dilute solution which can be directly used for spraying; s3, adjusting the pH value of the dilute solution which can be directly used for spraying to obtain a solution C; and S4, spraying and curing. The hydrogel coating prepared from the coating obtained by the method has the advantages of mild preparation conditions, no environmental pollution, capability of generating chemical bonding on various solid surfaces and the like; and the method for spraying the hydrogel coating is feasible, the preservation time is long, and the hydrogel coating can be sprayed on the surfaces of various substrate materials and can be stably bonded with a substrate.

Description

technical field [0001] The invention relates to the technical field of coatings, in particular to a sprayable hydrogel coating and a preparation method of the coating. Background technique [0002] Hydrogel is a kind of hydrophilic soft matter material formed by filling the polymer space network with aqueous solution. Due to their excellent biocompatibility, flexibility, and hydrophilic lubricity, hydrogel materials have broad application prospects in areas such as drug delivery, sensors, soft robots, medical devices, and marine antifouling coatings. In the application research of hydrogel materials, combining hydrogel as a coating material with various traditional solids, such as: glass, metal, ceramics, rubber and plastics, can give the characteristics of the above hydrogel to traditional solids Surface, promote the in-depth application of traditional materials in the fields of biomedicine and engineering. [0003] The diversification of application fields puts forward h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D133/14C09D7/20C08F220/20C08F230/08C08F2/48
CPCC09D143/04C09D7/20C08F220/20C08F2/48C08F230/085
Inventor 姚晰刘翠萍
Owner HENAN UNIVERSITY
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