Bio-based air purification nanofiber membrane for mask and preparation method
A nanofiber membrane and air purification technology, applied in the field of medical and sanitary materials, can solve the problems of mask protection effect, use comfort and poor mechanical properties, etc., and achieve the effect of good air purification effect, good protection effect and good mechanical performance.
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Embodiment 1
[0038] A method for preparing a bio-based air-purifying nanofiber membrane for face masks, first using rice husk powder, graphene-nano ceria composite powder, polyvinyl alcohol, and Polygonum cuspidatum root extract as raw materials to make a core layer solution or shell Layer solution, and then make nanofibrous film by coaxial electrospinning; Wherein, the preparation method of shell layer solution is as follows:
[0039] (1) Pretreat the fresh Polygonum cuspidatum root to make Polygonum cuspidatum root slurry, inoculate Lactobacillus plantarum, ferment and filter to obtain a fermentation liquid, then extract the fermentation liquid through a liquid membrane to obtain an extract of Polygonum cuspidatum root, and set aside;
[0040] (2) 1kg polyvinyl alcohol is then dissolved in 4kg water to obtain an aqueous solution;
[0041] (3) Dissolve 0.1kg cetyltrimethylammonium bromide in 8kg methanol, continue to add 4kg rice husk powder, 0.01kg graphene-nanometer ceria composite powd...
Embodiment 2
[0055] A method for preparing a bio-based air-purifying nanofiber membrane for face masks, first using rice husk powder, graphene-nano ceria composite powder, polyvinyl alcohol, and Polygonum cuspidatum root extract as raw materials to make a core layer solution or shell Layer solution, and then make nanofibrous film by coaxial electrospinning; Wherein, the preparation method of shell layer solution is as follows:
[0056] (1) Pretreat the fresh Polygonum cuspidatum root to make Polygonum cuspidatum root slurry, inoculate Lactobacillus plantarum, ferment and filter to obtain a fermentation liquid, then extract the fermentation liquid through a liquid membrane to obtain an extract of Polygonum cuspidatum root, and set aside;
[0057] (2) 1kg polyvinyl alcohol is then dissolved in 5kg water to obtain an aqueous solution;
[0058] (3) Dissolve 0.08kg cetyltrimethylammonium bromide in 10kg methanol again, continue to add 3kg rice husk powder, 0.02kg graphene-nanometer ceria compos...
Embodiment 3
[0072] A method for preparing a bio-based air-purifying nanofiber membrane for face masks, first using rice husk powder, graphene-nano ceria composite powder, polyvinyl alcohol, and Polygonum cuspidatum root extract as raw materials to make a core layer solution or shell Layer solution, and then make nanofibrous film by coaxial electrospinning; Wherein, the preparation method of shell layer solution is as follows:
[0073] (1) Pretreat the fresh Polygonum cuspidatum root to make Polygonum cuspidatum root slurry, inoculate Lactobacillus plantarum, ferment and filter to obtain a fermentation liquid, then extract the fermentation liquid through a liquid membrane to obtain an extract of Polygonum cuspidatum root, and set aside;
[0074] (2) 1kg polyvinyl alcohol is then dissolved in 4.5kg water to obtain an aqueous solution;
[0075] (3) 0.09kg cetyltrimethylammonium bromide is dissolved in 9kg methanol again, continue to add 3.5kg rice husk powder, 0.015kg graphene-nanometer ceri...
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